1-{(1S,2S)-3-(benzyloxy)-2-[di(4-methoxybenzyl)amino]-1-[(1,2:3,4-di-O-isopropylidene-6-deoxy-α-L-galactopyranos-6-yl)carbamoyl]propyl} 4-methyl succinate

Base Information

• Chemical Name: 1-{(1S,2S)-3-(benzyloxy)-2-[di(4-methoxybenzyl)amino]-1-[(1,2:3,4-di-O-isopropylidene-6-deoxy-α-L-galactopyranos-6-yl)carbamoyl]propyl} 4-methyl succinate
• CAS No.: 1006369-97-6
• Molecular Formula: C₄₄H₅₆N₂O₁₃
• Molecular Weight: 820.934

Synonyms:1-{(1S,2S)-3-(benzyloxy)-2-[di(4-methoxybenzyl)amino]-1-[(1,2:3,4-di-O-isopropylidene-6-deoxy-α-L-galactopyranos-6-yl)carbamoyl]propyl} 4-methyl succinate

Chemical Property of 1-{(1S,2S)-3-(benzyloxy)-2-[di(4-methoxybenzyl)amino]-1-[(1,2:3,4-di-O-isopropylidene-6-deoxy-α-L-galactopyranos-6-yl)carbamoyl]propyl} 4-methyl succinate

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Technology Process of 1-{(1S,2S)-3-(benzyloxy)-2-[di(4-methoxybenzyl)amino]-1-[(1,2:3,4-di-O-isopropylidene-6-deoxy-α-L-galactopyranos-6-yl)carbamoyl]propyl} 4-methyl succinate

There total 1 articles about 1-{(1S,2S)-3-(benzyloxy)-2-[di(4-methoxybenzyl)amino]-1-[(1,2:3,4-di-O-isopropylidene-6-deoxy-α-L-galactopyranos-6-yl)carbamoyl]propyl} 4-methyl succinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

N1-(1,2:3,4-di-O-isopropylidene-6-deoxy-α-L-galactopyranos-6-yl)-(2S,3S)-4-(benzyloxy)-3-[di(4-methoxybenzyl)amino]-2-hydroxybutanamide (1006369-94-3) + succinic acid monomethylester chloride (1490-25-1) → 1-{(1S,2S)-3-(benzyloxy)-2-[di(4-methoxybenzyl)amino]-1-[(1,2:3,4-di-O-isopropylidene-6-deoxy-α-L-galactopyranos-6-yl)carbamoyl]propyl} 4-methyl succinate (1006369-97-6)

Guidance literature:

With pyridine; In dichloromethane; at 0 - 20 ℃;

DOI:10.1016/j.carres.2007.10.001

Reference yield: 90.0%

1-{(1S,2S)-3-(benzyloxy)-2-[di(4-methoxybenzyl)amino]-1-[(1,2:3,4-di-O-isopropylidene-6-deoxy-α-L-galactopyranos-6-yl)carbamoyl]propyl} 4-methyl succinate (1006369-97-6) → methyl 3-{[(1S,2S)-1-[(benzyloxy)methyl]-2-hydroxy-2-[(1,2:3,4-di-O-isopropylidene-6-deoxy-α-L-galactopyranos-6-yl)carbamoyl]ethyl]carbamoyl}propanoate (1006370-00-8)

Guidance literature:

With ammonium cerium(IV) nitrate; In acetonitrile; at 0 - 20 ℃;

DOI:10.1016/j.carres.2007.10.001

upstream raw materials:

N1-(1,2:3,4-di-O-isopropylidene-6-deoxy-α-L-galactopyranos-6-yl)-(2S,3S)-4-(benzyloxy)-3-[di(4-methoxybenzyl)amino]-2-hydroxybutanamide

succinic acid monomethylester chloride

Downstream raw materials:

methyl 3-{[(1S,2S)-1-[(benzyloxy)methyl]-2-hydroxy-2-[(1,2:3,4-di-O-isopropylidene-6-deoxy-α-L-galactopyranos-6-yl)carbamoyl]ethyl]carbamoyl}propanoate

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