1,2:3,4-di-O-isopropylidene-6-O-[3-(2-methyl-4-nitroimidazolyl)-2-(4-trifluoromethoxy)benzyloxypropyl]-α-D-galactopyranose

Base Information

Chemical Name:1,2:3,4-di-O-isopropylidene-6-O-[3-(2-methyl-4-nitroimidazolyl)-2-(4-trifluoromethoxy)benzyloxypropyl]-α-D-galactopyranose
CAS No.:1333220-37-3
Molecular Formula:C₂₇H₃₄F₃N₃O₁₀
Molecular Weight:617.576
Hs Code.:

Synonyms:1,2:3,4-di-O-isopropylidene-6-O-[3-(2-methyl-4-nitroimidazolyl)-2-(4-trifluoromethoxy)benzyloxypropyl]-α-D-galactopyranose

Suppliers and Price of 1,2:3,4-di-O-isopropylidene-6-O-[3-(2-methyl-4-nitroimidazolyl)-2-(4-trifluoromethoxy)benzyloxypropyl]-α-D-galactopyranose

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1,2:3,4-di-O-isopropylidene-6-O-[3-(2-methyl-4-nitroimidazolyl)-2-(4-trifluoromethoxy)benzyloxypropyl]-α-D-galactopyranose

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1,2:3,4-di-O-isopropylidene-6-O-[3-(2-methyl-4-nitroimidazolyl)-2-(4-trifluoromethoxy)benzyloxypropyl]-α-D-galactopyranose

There total 3 articles about 1,2:3,4-di-O-isopropylidene-6-O-[3-(2-methyl-4-nitroimidazolyl)-2-(4-trifluoromethoxy)benzyloxypropyl]-α-D-galactopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1333220-26-0
6-O-[2-hydroxy-3-(2-methyl-4-nitroimidazolyl)propyl]-1,2:3,4-di-O-isopropylidene-α-D-galactopyranose

: 50824-05-0
4-trifluoromethoxybenzyl bromide

: 1333220-37-3
1,2:3,4-di-O-isopropylidene-6-O-[3-(2-methyl-4-nitroimidazolyl)-2-(4-trifluoromethoxy)benzyloxypropyl]-α-D-galactopyranose

Guidance literature:: 6-O-[2-hydroxy-3-(2-methyl-4-nitroimidazolyl)propyl]-1,2:3,4-di-O-isopropylidene-α-D-galactopyranose; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 0.25h;

4-trifluoromethoxybenzyl bromide; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; for 5h;
DOI:10.1016/j.ejmech.2011.05.045

Reference yield:

: 4064-06-6
1,2:3,4-di-O-isopropylidene-α-D-galactopyranose

: 1333220-37-3
1,2:3,4-di-O-isopropylidene-6-O-[3-(2-methyl-4-nitroimidazolyl)-2-(4-trifluoromethoxy)benzyloxypropyl]-α-D-galactopyranose

Guidance literature:: Multi-step reaction with 3 steps

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.25 h / 0 °C

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.25 h / 0 °C

3.2: 5 h / 0 - 20 °C

With sodium hydride; In N,N-dimethyl-formamide; mineral oil;
DOI:10.1016/j.ejmech.2011.05.045

Reference yield:

: 70969-90-3,134876-99-6,134930-14-6
6-O-[(2R,S)-2,3-epoxypropyl]-1,2:3,4-di-O-isopropylidene-α-D-galactopyranose

: 1333220-37-3
1,2:3,4-di-O-isopropylidene-6-O-[3-(2-methyl-4-nitroimidazolyl)-2-(4-trifluoromethoxy)benzyloxypropyl]-α-D-galactopyranose

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.25 h / 0 °C

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.25 h / 0 °C

2.2: 5 h / 0 - 20 °C

With sodium hydride; In N,N-dimethyl-formamide; mineral oil;
DOI:10.1016/j.ejmech.2011.05.045