(D)-2,3:5,6-di-O-cyclohexylidene 1-[(2S,4R,5S)-3,4-dimethyl-5-phenyl-2-sulfide-1,3,2-oxazaphospholidinyl]myo-inositol

Base Information

• Chemical Name: (D)-2,3:5,6-di-O-cyclohexylidene 1-[(2S,4R,5S)-3,4-dimethyl-5-phenyl-2-sulfide-1,3,2-oxazaphospholidinyl]myo-inositol
• CAS No.: 248585-26-4
• Molecular Formula: C₂₈H₄₀NO₇PS
• Molecular Weight: 565.668

Synonyms:(D)-2,3:5,6-di-O-cyclohexylidene 1-[(2S,4R,5S)-3,4-dimethyl-5-phenyl-2-sulfide-1,3,2-oxazaphospholidinyl]myo-inositol

Chemical Property of (D)-2,3:5,6-di-O-cyclohexylidene 1-[(2S,4R,5S)-3,4-dimethyl-5-phenyl-2-sulfide-1,3,2-oxazaphospholidinyl]myo-inositol

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Technology Process of (D)-2,3:5,6-di-O-cyclohexylidene 1-[(2S,4R,5S)-3,4-dimethyl-5-phenyl-2-sulfide-1,3,2-oxazaphospholidinyl]myo-inositol

There total 1 articles about (D)-2,3:5,6-di-O-cyclohexylidene 1-[(2S,4R,5S)-3,4-dimethyl-5-phenyl-2-sulfide-1,3,2-oxazaphospholidinyl]myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(±)-1,2:4,5-di-O-cyclohexylidene-myo-inositol + (2R,4R,5S)-(+)-2-chloro-3,4-dimethyl-5-phenyl-1,3,2-oxazaphospholidine-2-sulfide → (D)-2,3:5,6-di-O-cyclohexylidene 1-[(2S,4R,5S)-3,4-dimethyl-5-phenyl-2-sulfide-1,3,2-oxazaphospholidinyl]myo-inositol (248585-26-4) + (D)-1,2:4,5-di-O-cyclohexylidene 3-[(2S,4R,5S)-3,4-dimethyl-5-phenyl-2-sulfide-1,3,2-oxazaphospholidinyl]myo-inositol

Guidance literature:

(±)-1,2:4,5-di-O-cyclohexylidene-myo-inositol; With sodium hydride; In N,N-dimethyl-formamide; at 1 ℃; for 0h;

(2R,4R,5S)-(+)-2-chloro-3,4-dimethyl-5-phenyl-1,3,2-oxazaphospholidine-2-sulfide; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 2h; Further stages.;

DOI:10.1021/jm011056m

Reference yield:

(D)-2,3:5,6-di-O-cyclohexylidene 1-[(2S,4R,5S)-3,4-dimethyl-5-phenyl-2-sulfide-1,3,2-oxazaphospholidinyl]myo-inositol (248585-26-4) → C16H26NO7(17)OPS

Guidance literature:

With trifluoroacetic anhydride; ¹⁷O-water; In tetrahydrofuran;

DOI:10.1021/ja991939r

Reference yield:

(D)-2,3:5,6-di-O-cyclohexylidene 1-[(2S,4R,5S)-3,4-dimethyl-5-phenyl-2-sulfide-1,3,2-oxazaphospholidinyl]myo-inositol (248585-26-4) → (R)-Thiophosphoric acid O-((1S,2R)-2-methylamino-1-phenyl-propyl) ester O'-((1R,2S,3R,4R,5R,6R)-2,3,4,5,6-pentahydroxy-cyclohexyl) ester + (R)-Thiophosphoric acid O-((1S,2R)-2-methylamino-1-phenyl-propyl) ester O'-((1R,2S,3S,4R,5S,6R)-2,3,4,5,6-pentahydroxy-cyclohexyl) ester + (R)-Thiophosphoric acid O-((1S,2R)-2-methylamino-1-phenyl-propyl) ester O'-((1S,2S,3R,4S,5S,6S)-2,3,4,5,6-pentahydroxy-cyclohexyl) ester + (1S,2R)-(2-methylamino-1-phenylpropyl) 1-myo-inositol-(Rp)-[16O,17O]-thiophosphate

Guidance literature:

With water; trifluoroacetic anhydride; ¹⁷O-water; In tetrahydrofuran; at 5 ℃; for 0.5h; Title compound not separated from byproducts.;

DOI:10.1021/jm011056m

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