Technology Process of sulfido bis(2,6-diisopropylphenyl)phenylphosphane
There total 4 articles about sulfido bis(2,6-diisopropylphenyl)phenylphosphane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sulfur;
In
5,5-dimethyl-1,3-cyclohexadiene;
at 110 ℃;
for 17h;
Inert atmosphere;
DOI:10.1021/ja403555d
- Guidance literature:
-
Multi-step reaction with 4 steps
1: tetrahydrofuran / -70 - 20 °C / Inert atmosphere
2: 5,5-dimethyl-1,3-cyclohexadiene / 20 h / Inert atmosphere; Reflux
3: ammonia / 5,5-dimethyl-1,3-cyclohexadiene; water / Inert atmosphere
4: sulfur / 5,5-dimethyl-1,3-cyclohexadiene / 17 h / 110 °C / Inert atmosphere
With
sulfur; ammonia;
In
tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene; water;
DOI:10.1021/ja403555d
- Guidance literature:
-
Multi-step reaction with 2 steps
1: ammonia / 5,5-dimethyl-1,3-cyclohexadiene; water / Inert atmosphere
2: sulfur / 5,5-dimethyl-1,3-cyclohexadiene / 17 h / 110 °C / Inert atmosphere
With
sulfur; ammonia;
In
5,5-dimethyl-1,3-cyclohexadiene; water;
DOI:10.1021/ja403555d
