C₃₄H₄₀INO₃

Base Information

Chemical Name:C₃₄H₄₀INO₃
CAS No.:954096-37-8
Molecular Formula:C₃₄H₄₀INO₃
Molecular Weight:637.601
Hs Code.:

C<sub>34</sub>H<sub>40</sub>INO<sub>3</sub>

Synonyms:C₃₄H₄₀INO₃

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Chemical Property of C₃₄H₄₀INO₃

Chemical Property:

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Technology Process of C₃₄H₄₀INO₃

There total 10 articles about C₃₄H₄₀INO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 954096-36-7
C₃₃H₃₉IO₃

: 151-50-8
potassium cyanide

: 954096-37-8
C₃₄H₄₀INO₃

: C₃₄H₄₀INO₃

: C₃₄H₄₀INO₃

Guidance literature:: In N,N-dimethyl-formamide; at 100 ℃; for 24h;
DOI:10.1016/j.tetlet.2007.07.179

Reference yield:

: 954096-35-6
C₃₃H₄₁IO₃

: 954096-37-8
C₃₄H₄₀INO₃

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / IBX / dimethylsulfoxide / 4 h / 70 °C

2: 70 percent / dimethylformamide / 24 h / 100 °C

With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2007.07.179

Reference yield:

: 954096-34-5
C₁₇H₂₁IO₂

: 954096-37-8
C₃₄H₄₀INO₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: nBuLi / tetrahydrofuran / 0.25 h / -78 °C

1.2: 99 percent / tetrahydrofuran / 1 h

2.1: 97 percent / IBX / dimethylsulfoxide / 4 h / 70 °C

3.1: 70 percent / dimethylformamide / 24 h / 100 °C

With n-butyllithium; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2007.07.179