(S)-tert-butyl (2-phenyl-1-(3-phenyl-1H-1,2,4-triazol-5-yl)ethyl)carbamate

Base Information

Chemical Name:(S)-tert-butyl (2-phenyl-1-(3-phenyl-1H-1,2,4-triazol-5-yl)ethyl)carbamate
CAS No.:872017-66-8
Molecular Formula:C₂₁H₂₄N₄O₂
Molecular Weight:364.447
Hs Code.:

Synonyms:(S)-tert-butyl (2-phenyl-1-(3-phenyl-1H-1,2,4-triazol-5-yl)ethyl)carbamate

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Chemical Property of (S)-tert-butyl (2-phenyl-1-(3-phenyl-1H-1,2,4-triazol-5-yl)ethyl)carbamate

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Technology Process of (S)-tert-butyl (2-phenyl-1-(3-phenyl-1H-1,2,4-triazol-5-yl)ethyl)carbamate

There total 3 articles about (S)-tert-butyl (2-phenyl-1-(3-phenyl-1H-1,2,4-triazol-5-yl)ethyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 30189-48-1
C₁₄H₂₁N₃O₃

: 5333-86-8
ethyl benzimidate hydrochloride

: 872017-66-8
(S)-tert-butyl (2-phenyl-1-(3-phenyl-1H-1,2,4-triazol-5-yl)ethyl)carbamate

Guidance literature:: With triethylamine; In acetonitrile; for 24h; Heating / reflux;

Reference yield: 42.0%

: 5333-86-8
ethyl benzimidate hydrochloride

: 30189-48-1
(S)-tert-butyl (1-hydrazinyl-1-oxo-3-phenylpropan-2-yl)carbamate

: 872017-66-8
(S)-tert-butyl (2-phenyl-1-(3-phenyl-1H-1,2,4-triazol-5-yl)ethyl)carbamate

Guidance literature:: With triethylamine; In acetonitrile; for 24h; Inert atmosphere; Reflux;
DOI:10.1021/jm5010607

Reference yield:

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 872017-66-8
(S)-tert-butyl (2-phenyl-1-(3-phenyl-1H-1,2,4-triazol-5-yl)ethyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; pyridine / 16 h / 20 °C / Inert atmosphere

2: triethylamine / acetonitrile / 24 h / Inert atmosphere; Reflux

With pyridine; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine; hydrazine; In acetonitrile;
DOI:10.1021/jm5010607