3,3'-[butane-1,4-diylbis(carbonyliminocarbonothioylimino)]bis[benzoic acid chloride]

Base Information

Chemical Name:3,3'-[butane-1,4-diylbis(carbonyliminocarbonothioylimino)]bis[benzoic acid chloride]
CAS No.:1263194-88-2
Molecular Formula:C₂₂H₂₀Cl₂N₄O₄S₂
Molecular Weight:539.463
Hs Code.:

Synonyms:3,3'-[butane-1,4-diylbis(carbonyliminocarbonothioylimino)]bis[benzoic acid chloride]

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Chemical Property of 3,3'-[butane-1,4-diylbis(carbonyliminocarbonothioylimino)]bis[benzoic acid chloride]

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Technology Process of 3,3'-[butane-1,4-diylbis(carbonyliminocarbonothioylimino)]bis[benzoic acid chloride]

There total 3 articles about 3,3'-[butane-1,4-diylbis(carbonyliminocarbonothioylimino)]bis[benzoic acid chloride] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1263194-85-9
3,3'-[butane-1,4-diylbis(carbonyliminocarbonothioylimino)]bis[benzoic acid]

: 1263194-88-2
3,3'-[butane-1,4-diylbis(carbonyliminocarbonothioylimino)]bis[benzoic acid chloride]

Guidance literature:: With thionyl chloride; at 35 ℃; for 168h;
DOI:10.1007/s00706-010-0422-1

Reference yield:

: 111-50-2
Adipic acid dichloride

: 1263194-88-2
3,3'-[butane-1,4-diylbis(carbonyliminocarbonothioylimino)]bis[benzoic acid chloride]

Guidance literature:: Multi-step reaction with 3 steps

1: benzene / 6 h / 110 - 120 °C / Reflux

2: dichloromethane / 1 h / 0 °C / Inert atmosphere

3: thionyl chloride / 168 h / 35 °C

With thionyl chloride; In dichloromethane; benzene;
DOI:10.1007/s00706-010-0422-1

Reference yield:

: 7710-11-4
adipoyl isothiocyanate

: 1263194-88-2
3,3'-[butane-1,4-diylbis(carbonyliminocarbonothioylimino)]bis[benzoic acid chloride]

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 1 h / 0 °C / Inert atmosphere

2: thionyl chloride / 168 h / 35 °C

With thionyl chloride; In dichloromethane;
DOI:10.1007/s00706-010-0422-1