ethyl 2-{[(2R)-2-[(tert-butylsulfinyl)amino]-2-(3,5-difluorophenyl)ethyl]thio}-2-methylpropanoate

Base Information

Chemical Name:ethyl 2-{[(2R)-2-[(tert-butylsulfinyl)amino]-2-(3,5-difluorophenyl)ethyl]thio}-2-methylpropanoate
CAS No.:957121-24-3
Molecular Formula:C₁₈H₂₇F₂NO₃S₂
Molecular Weight:407.546
Hs Code.:

Synonyms:ethyl 2-{[(2R)-2-[(tert-butylsulfinyl)amino]-2-(3,5-difluorophenyl)ethyl]thio}-2-methylpropanoate

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Chemical Property of ethyl 2-{[(2R)-2-[(tert-butylsulfinyl)amino]-2-(3,5-difluorophenyl)ethyl]thio}-2-methylpropanoate

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Technology Process of ethyl 2-{[(2R)-2-[(tert-butylsulfinyl)amino]-2-(3,5-difluorophenyl)ethyl]thio}-2-methylpropanoate

There total 1 articles about ethyl 2-{[(2R)-2-[(tert-butylsulfinyl)amino]-2-(3,5-difluorophenyl)ethyl]thio}-2-methylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: titanium(IV) tetraethanolate

: 957121-23-2
methyl 2-{[2-(3,5-difluorophenyl)-2-oxoethyl]thio}-2-methylpropanoate

: 196929-78-9
(R)-2-methylpropane-2-sulfinamide

: 957121-24-3
ethyl 2-{[(2R)-2-[(tert-butylsulfinyl)amino]-2-(3,5-difluorophenyl)ethyl]thio}-2-methylpropanoate

: ethyl 2-{[(2S)-2-[(tert-butylsulfinyl)amino]-2-(3,5-difluorophenyl)ethyl]thio}-2-methylpropanoate

Guidance literature:: titanium(IV) tetraethanolate; methyl 2-{[2-(3,5-difluorophenyl)-2-oxoethyl]thio}-2-methylpropanoate; (R)-2-methylpropane-2-sulfinamide; In tetrahydrofuran; at 60 ℃; for 15h; Sealed vessel;

With sodium tetrahydroborate; In tetrahydrofuran; at 0 ℃; for 0.25h;

Reference yield:

: 957121-24-3
ethyl 2-{[(2R)-2-[(tert-butylsulfinyl)amino]-2-(3,5-difluorophenyl)ethyl]thio}-2-methylpropanoate

: 957121-20-9
(5R)-5-(3,5-difluorophenyl)-2,2-dimethylthiomorpholin-3-one

Guidance literature:: ethyl 2-{[(2R)-2-[(tert-butylsulfinyl)amino]-2-(3,5-difluorophenyl)ethyl]thio}-2-methylpropanoate; With hydrogenchloride; In methanol; at 0 ℃; for 0.25h; Sealed vessel;

With triethylamine; In methanol; toluene; at 115 ℃; for 168h; Heating / reflux;