Technology Process of 4-[(3-methyl-1,2-benzisoxazol-4-yl)oxy]aniline
There total 5 articles about 4-[(3-methyl-1,2-benzisoxazol-4-yl)oxy]aniline which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
3-methyl-4-[(4-nitrophenyl)oxy]-1,2-benzisoxazole;
With
tin(II) chloride dihdyrate; ethanol;
at 90 ℃;
for 5h;
Inert atmosphere;
With
sodium hydrogencarbonate;
In
water; ethyl acetate;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 2.5 h / Reflux; Inert atmosphere
2: 0.25 h / 20 °C
3: pyridine / 2 h / Reflux
4: potassium carbonate / N,N-dimethyl-formamide / 1 h / 110 °C / Microwave irradiation
5: ethanol; tin(II) chloride dihdyrate / 5 h / 90 °C / Inert atmosphere
With
pyridine; tin(II) chloride dihdyrate; ethanol; hydroxylamine hydrochloride; sodium acetate; potassium carbonate;
In
ethanol; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 110 °C / Microwave irradiation
2: ethanol; tin(II) chloride dihdyrate / 5 h / 90 °C / Inert atmosphere
With
tin(II) chloride dihdyrate; ethanol; potassium carbonate;
In
N,N-dimethyl-formamide;
![3-methyl-4-[(4-nitrophenyl)oxy]-1,2-benzisoxazole](/Databaselist/images/loading.webp)
