α-bromohexanophenone

Base Information

• Chemical Name: α-bromohexanophenone
• CAS No.: 59774-06-0
• Molecular Formula: C₁₂H₁₅BrO
• Molecular Weight: 255.155
• Mol file: 59774-06-0.mol

Synonyms:α-bromohexanophenone

Chemical Property of α-bromohexanophenone

Chemical Property:

• Boiling Point: 98 °C(Press: 0.3 Torr)
• Density: 1.272±0.06 g/cm3(Predicted)

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: This product is sold as designer drug on the illicit drug market.

Technology Process of α-bromohexanophenone

There total 9 articles about α-bromohexanophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

hexylbenzene (1077-16-3) → α-bromohexanophenone (59774-06-0)

Guidance literature:

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); water; In ethyl acetate; at 60 ℃; for 6h;

DOI:10.1002/ejoc.201900100

Reference yield: 77.0%

1-phenylhexan-1-ol (4471-05-0) → α-bromohexanophenone (59774-06-0)

Guidance literature:

With hydrogen bromide; dihydrogen peroxide; In water; acetonitrile; at 65 - 70 ℃; for 6h; Green chemistry;

DOI:10.1039/c8ra04885a

Reference yield: 64.0%

2-bromohexanoyl bromide (54971-26-5,38532-59-1) + benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → α-bromohexanophenone (59774-06-0)

Guidance literature:

With aluminium trichloride; In dichloromethane; for 12h;

DOI:10.1039/DT9950000587

upstream raw materials:

caprophenone

benzoic acid methyl ester

1,1-dibromopentane

2-bromohexanoyl bromide

Downstream raw materials:

5-butyl-4-phenyl-oxazol-2-ylamine

4-butyl-5-phenyl-1,3-dihydro-imidazol-2-one

2-Hydroxy-1-phenyl-1-hexanone

tetrahydro-3-butyl-2-hydroxy-4-(2-hydroxyethyl)-2-phenyl-2H-1,4-oxazine