4-[2'-{(5''-bromopentyl)oxy}ethyl]1,2-dibenzyloxybenzene

Base Information

Chemical Name:4-[2'-{(5''-bromopentyl)oxy}ethyl]1,2-dibenzyloxybenzene
CAS No.:178486-13-0
Molecular Formula:C₂₇H₃₁BrO₃
Molecular Weight:483.445
Hs Code.:

Synonyms:4-[2'-{(5''-bromopentyl)oxy}ethyl]1,2-dibenzyloxybenzene

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Chemical Property of 4-[2'-{(5''-bromopentyl)oxy}ethyl]1,2-dibenzyloxybenzene

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Technology Process of 4-[2'-{(5''-bromopentyl)oxy}ethyl]1,2-dibenzyloxybenzene

There total 4 articles about 4-[2'-{(5''-bromopentyl)oxy}ethyl]1,2-dibenzyloxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 111-24-0
1,5-dibromo-pentane

: 96826-11-8
2-<3,4-bis(benzyloxy)phenyl>ethanol

: 178486-13-0
4-[2'-{(5''-bromopentyl)oxy}ethyl]1,2-dibenzyloxybenzene

Guidance literature:: With sodium hydride; In dimethyl sulfoxide; at 20 ℃; for 5h; Inert atmosphere;
DOI:10.1016/j.ejmech.2019.07.053

Reference yield:

: 111-24-0
1,5-dibromo-pentane

: 96826-11-8
2-<3,4-bis(benzyloxy)phenyl>ethanol

: 178486-12-9
6-[2-[3,4-di(phenylmethoxy)phenyl]ethoxy]hexanoic acid

: 178486-13-0
4-[2'-{(5''-bromopentyl)oxy}ethyl]1,2-dibenzyloxybenzene

Guidance literature:: With NaH; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

: 100-44-7
benzyl chloride

: 178486-13-0
4-[2'-{(5''-bromopentyl)oxy}ethyl]1,2-dibenzyloxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 5 h / 65 °C

2: sodium hydride / N,N-dimethyl-formamide / 10 h / 20 °C / Inert atmosphere

With sodium hydride; potassium carbonate; In N,N-dimethyl-formamide; 2: |Williamson Ether Synthesis;
DOI:10.1016/j.ejmech.2021.113980