methyl -12-(phenylthio)-9-octadecenoate

Base Information

Chemical Name:methyl -12-(phenylthio)-9-octadecenoate
CAS No.:123053-52-1
Molecular Formula:C₂₅H₄₀O₂S
Molecular Weight:404.657
Hs Code.:

methyl <S-(E)>-12-(phenylthio)-9-octadecenoate

Synonyms:methyl -12-(phenylthio)-9-octadecenoate

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Chemical Property of methyl -12-(phenylthio)-9-octadecenoate

Chemical Property:

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Technology Process of methyl -12-(phenylthio)-9-octadecenoate

There total 5 articles about methyl -12-(phenylthio)-9-octadecenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

: ((E)-(S)-11-Carboxy-1-hexyl-undec-3-enyl)-methyl-phenyl-sulfonium; perchlorate

: 59744-10-4
(-)-(R,E)-12-hydroxy-9-octadecenoic acid lactone

: 69651-29-2
(+)-S-trans-12-hydrohy-9-octadecenoic acid lactone

: 123053-52-1
methyl -12-(phenylthio)-9-octadecenoate

Guidance literature:: With potassium carbonate; In acetonitrile; for 36h; Yields of byproduct given; Heating;
DOI:10.1021/jo00283a010

Reference yield:

: 540-12-5,27925-02-6,7431-95-0,84799-84-8
ricinelaidic acid

: 123053-52-1
methyl -12-(phenylthio)-9-octadecenoate

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / diethyl ether

2: 58 percent / pyridine / 40 h / Ambient temperature

3: 1.) sodium, methanol / 1.) RT, 30 min, 2.) MeOH, reflux, 3 h

With pyridine; methanol; sodium; In diethyl ether;
DOI:10.1021/jo00283a010

Reference yield:

: 141-22-0,27925-02-6,7431-95-0,84799-84-8
Ricinoleic acid

: 123053-52-1
methyl -12-(phenylthio)-9-octadecenoate

Guidance literature:: Multi-step reaction with 4 steps

1: 34 percent / Ph₂S₂ / hexane / Irradiation

2: 95 percent / diethyl ether

3: 58 percent / pyridine / 40 h / Ambient temperature

4: 1.) sodium, methanol / 1.) RT, 30 min, 2.) MeOH, reflux, 3 h

With pyridine; methanol; sodium; diphenyldisulfane; In diethyl ether; hexane;
DOI:10.1021/jo00283a010