Methyl 3-hydroxy-2,2-dimethyl-4-(p-methoxyphenyl)imino-3-phenylbutanoate

Base Information

Chemical Name:Methyl 3-hydroxy-2,2-dimethyl-4-(p-methoxyphenyl)imino-3-phenylbutanoate
CAS No.:131856-80-9
Molecular Formula:C₂₀H₂₃NO₄
Molecular Weight:341.407
Hs Code.:

Synonyms:Methyl 3-hydroxy-2,2-dimethyl-4-(p-methoxyphenyl)imino-3-phenylbutanoate

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Chemical Property of Methyl 3-hydroxy-2,2-dimethyl-4-(p-methoxyphenyl)imino-3-phenylbutanoate

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Technology Process of Methyl 3-hydroxy-2,2-dimethyl-4-(p-methoxyphenyl)imino-3-phenylbutanoate

There total 4 articles about Methyl 3-hydroxy-2,2-dimethyl-4-(p-methoxyphenyl)imino-3-phenylbutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 109685-15-6,109685-32-7
3-Hydroxy-4-methoxy-4-(4-methoxy-phenylamino)-2,2-dimethyl-3-phenyl-butyric acid methyl ester

: 131856-80-9
Methyl 3-hydroxy-2,2-dimethyl-4-(p-methoxyphenyl)imino-3-phenylbutanoate

Guidance literature:: In chloroform; for 2h; Ambient temperature;
DOI:10.1016/S0040-4020(01)87868-6

Reference yield:

: 547-63-7,133320-07-7,67505-84-4
Methyl isobutyrate

: 131856-80-9
Methyl 3-hydroxy-2,2-dimethyl-4-(p-methoxyphenyl)imino-3-phenylbutanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) lithium diisopropylamide / 1.) THF, hexanes, -78 deg C, 15 min, 2.) -78 deg C, 5 min

2: 79 percent / CHCl₃ / 2 h / Ambient temperature

With lithium diisopropyl amide; In chloroform;
DOI:10.1016/S0040-4020(01)87868-6

Reference yield:

: 91851-03-5
4-methoxy-N-(α-methoxyphenacyl)aniline

: 131856-80-9
Methyl 3-hydroxy-2,2-dimethyl-4-(p-methoxyphenyl)imino-3-phenylbutanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) lithium diisopropylamide / 1.) THF, hexanes, -78 deg C, 15 min, 2.) -78 deg C, 5 min

2: 79 percent / CHCl₃ / 2 h / Ambient temperature

With lithium diisopropyl amide; In chloroform;
DOI:10.1016/S0040-4020(01)87868-6