1-O-phyllanthocinoyl 3-O-(chloroacetyl)-4-O-acetyl-6-deoxy-2-O-(2,4-bis-O-(chloroacetyl)-3-O-acetyl-6-deoxy-β-D-glucopyranosyl)-α-D-glucopyranoside

Base Information

Chemical Name:1-O-phyllanthocinoyl 3-O-(chloroacetyl)-4-O-acetyl-6-deoxy-2-O-(2,4-bis-O-(chloroacetyl)-3-O-acetyl-6-deoxy-β-D-glucopyranosyl)-α-D-glucopyranoside
CAS No.:114828-04-5
Molecular Formula:C₄₆H₅₅Cl₃O₂₀
Molecular Weight:1034.29
Hs Code.:

1-O-phyllanthocinoyl 3-O-(chloroacetyl)-4-O-acetyl-6-deoxy-2-O-(2,4-bis-O-(chloroacetyl)-3-O-acetyl-6-deoxy-β-D-glucopyranosyl)-α-D-glucopyranoside

Synonyms:1-O-phyllanthocinoyl 3-O-(chloroacetyl)-4-O-acetyl-6-deoxy-2-O-(2,4-bis-O-(chloroacetyl)-3-O-acetyl-6-deoxy-β-D-glucopyranosyl)-α-D-glucopyranoside

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Chemical Property of 1-O-phyllanthocinoyl 3-O-(chloroacetyl)-4-O-acetyl-6-deoxy-2-O-(2,4-bis-O-(chloroacetyl)-3-O-acetyl-6-deoxy-β-D-glucopyranosyl)-α-D-glucopyranoside

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Technology Process of 1-O-phyllanthocinoyl 3-O-(chloroacetyl)-4-O-acetyl-6-deoxy-2-O-(2,4-bis-O-(chloroacetyl)-3-O-acetyl-6-deoxy-β-D-glucopyranosyl)-α-D-glucopyranoside

There total 3 articles about 1-O-phyllanthocinoyl 3-O-(chloroacetyl)-4-O-acetyl-6-deoxy-2-O-(2,4-bis-O-(chloroacetyl)-3-O-acetyl-6-deoxy-β-D-glucopyranosyl)-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

: 114828-03-4
C₂₄H₂₈O₇

: 109922-63-6
3-O-(chloroacetyl)-4-O-acetyl-6-deoxy-2-O-(2,4-bis-O-(chloroacetyl)-3-O-acetyl-6-deoxy-β-D-glucopyranosyl)-α-D-glucopyranose

: 116135-14-9
C₃₂H₄₂N₂O₁₀

: 114828-04-5
1-O-phyllanthocinoyl 3-O-(chloroacetyl)-4-O-acetyl-6-deoxy-2-O-(2,4-bis-O-(chloroacetyl)-3-O-acetyl-6-deoxy-β-D-glucopyranosyl)-α-D-glucopyranoside

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; for 0.5h; Ambient temperature;

Reference yield:

: Chloro-acetic acid (2S,3R,4S,5R,6R)-4-acetoxy-2-[(3R,4S,5R,6R)-5-acetoxy-2-bromo-4-(2-chloro-acetoxy)-6-methyl-tetrahydro-pyran-3-yloxy]-5-(2-chloro-acetoxy)-6-methyl-tetrahydro-pyran-3-yl ester

: 114828-04-5
1-O-phyllanthocinoyl 3-O-(chloroacetyl)-4-O-acetyl-6-deoxy-2-O-(2,4-bis-O-(chloroacetyl)-3-O-acetyl-6-deoxy-β-D-glucopyranosyl)-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: H₂O, Ag₂CO₃ / acetone / 3 h

2: 61 percent / PPh₃, diisopropyl azodicarboxylate / tetrahydrofuran / 0.5 h / Ambient temperature

With di-isopropyl azodicarboxylate; water; triphenylphosphine; silver carbonate; In tetrahydrofuran; acetone;

Reference yield:

: 114828-01-2,131589-97-4
Chloro-acetic acid (3R,4S,5R,6R)-2,5-diacetoxy-3-[(2S,3R,4S,5R,6R)-4-acetoxy-3,5-bis-(2-chloro-acetoxy)-6-methyl-tetrahydro-pyran-2-yloxy]-6-methyl-tetrahydro-pyran-4-yl ester

: 114828-04-5
1-O-phyllanthocinoyl 3-O-(chloroacetyl)-4-O-acetyl-6-deoxy-2-O-(2,4-bis-O-(chloroacetyl)-3-O-acetyl-6-deoxy-β-D-glucopyranosyl)-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 30percent HBr / acetic acid / Ambient temperature

2: H₂O, Ag₂CO₃ / acetone / 3 h

3: 61 percent / PPh₃, diisopropyl azodicarboxylate / tetrahydrofuran / 0.5 h / Ambient temperature

With di-isopropyl azodicarboxylate; water; hydrogen bromide; triphenylphosphine; silver carbonate; In tetrahydrofuran; acetic acid; acetone;