4,9,13,17,22-pentatosyl-N¹,N²⁵-diformyl-4,9,13,17,22-pentaazapentacosane-1,25-diamine

Base Information

• Chemical Name: 4,9,13,17,22-pentatosyl-N¹,N²⁵-diformyl-4,9,13,17,22-pentaazapentacosane-1,25-diamine
• CAS No.: 121821-25-8
• Molecular Formula: C₅₇H₇₉N₇O₁₂S₅
• Molecular Weight: 1214.62

Synonyms:4,9,13,17,22-pentatosyl-N¹,N²⁵-diformyl-4,9,13,17,22-pentaazapentacosane-1,25-diamine

Chemical Property of 4,9,13,17,22-pentatosyl-N¹,N²⁵-diformyl-4,9,13,17,22-pentaazapentacosane-1,25-diamine

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Technology Process of 4,9,13,17,22-pentatosyl-N¹,N²⁵-diformyl-4,9,13,17,22-pentaazapentacosane-1,25-diamine

There total 1 articles about 4,9,13,17,22-pentatosyl-N¹,N²⁵-diformyl-4,9,13,17,22-pentaazapentacosane-1,25-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

N,N-dimethyl-formamide (68-12-2,33513-42-7) + 4,9,13,17,22-pentatosyl-N1,N1:N25,N25-diphthaloyl-4,9,13,17,22-pentaazapentacosane-1,25-diamine (121821-37-2) → 4,9,13,17,22-pentatosyl-N1,N25-diformyl-4,9,13,17,22-pentaazapentacosane-1,25-diamine (121821-25-8)

Guidance literature:

With hydrazine hydrate; at 75 ℃; for 23h;

DOI:10.1246/bcsj.62.198

Reference yield:

4,9,13,17,22-pentatosyl-N1,N25-diformyl-4,9,13,17,22-pentaazapentacosane-1,25-diamine (121821-25-8) → C55H79N7O10S5*2ClH

Guidance literature:

With hydrogenchloride; In ethanol; at 80 ℃; for 4h;

DOI:10.1246/bcsj.62.198

Reference yield:

4,9,13,17,22-pentatosyl-N1,N25-diformyl-4,9,13,17,22-pentaazapentacosane-1,25-diamine (121821-25-8) → N1,N25,4,9,13,17,22-heptatosyl-4,9,13,17,22-pentaazapentacosane-1,25-diamine

Guidance literature:

Multi-step reaction with 2 steps

1: 2M HCl / ethanol / 4 h / 80 °C

2: Et₃N, pyridine / 4 h / Ambient temperature

With pyridine; hydrogenchloride; triethylamine; In ethanol;

DOI:10.1246/bcsj.62.198

upstream raw materials:

N,N-dimethyl-formamide

4,9,13,17,22-pentatosyl-N¹,N¹:N²⁵,N²⁵-diphthaloyl-4,9,13,17,22-pentaazapentacosane-1,25-diamine

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