hexamethyleneammonium 2-<1-(4-bromophenyl)-2-thiocarbamoyl-2-cyanoethyl>-5,5-dimethyl-3-oxo-1-cyclohexen-1-olate

Base Information

Chemical Name:hexamethyleneammonium 2-<1-(4-bromophenyl)-2-thiocarbamoyl-2-cyanoethyl>-5,5-dimethyl-3-oxo-1-cyclohexen-1-olate
CAS No.:131270-67-2
Molecular Formula:C₆H₁₃N*C₁₈H₁₉BrN₂O₂S
Molecular Weight:506.507
Hs Code.:

Synonyms:hexamethyleneammonium 2-<1-(4-bromophenyl)-2-thiocarbamoyl-2-cyanoethyl>-5,5-dimethyl-3-oxo-1-cyclohexen-1-olate

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Chemical Property of hexamethyleneammonium 2-<1-(4-bromophenyl)-2-thiocarbamoyl-2-cyanoethyl>-5,5-dimethyl-3-oxo-1-cyclohexen-1-olate

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Technology Process of hexamethyleneammonium 2-<1-(4-bromophenyl)-2-thiocarbamoyl-2-cyanoethyl>-5,5-dimethyl-3-oxo-1-cyclohexen-1-olate

There total 7 articles about hexamethyleneammonium 2-<1-(4-bromophenyl)-2-thiocarbamoyl-2-cyanoethyl>-5,5-dimethyl-3-oxo-1-cyclohexen-1-olate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 111-49-9
hexamethylene imine

: 68029-54-9,95639-00-2
3-(4-bromophenyl)-2-cyanoprop-2-enethioamide

: 126-81-8
dimedone

: 131270-67-2
hexamethyleneammonium 2-<1-(4-bromophenyl)-2-thiocarbamoyl-2-cyanoethyl>-5,5-dimethyl-3-oxo-1-cyclohexen-1-olate

Guidance literature:: In ethanol; at 25 ℃; for 4h;

Reference yield: 85.0%

: 111-49-9
hexamethylene imine

: 68029-54-9
(E)-3-(4-bromophenyl)-2-cyanoprop-2-enethioamide

: 126-81-8
dimedone

: 131270-67-2
hexamethyleneammonium 2-<1-(4-bromophenyl)-2-thiocarbamoyl-2-cyanoethyl>-5,5-dimethyl-3-oxo-1-cyclohexen-1-olate

Guidance literature:: In ethanol; at 25 ℃; for 5h;

Reference yield:

: 117822-61-4
3-(5,5-dimethyl-1-hydroxy-3-oxo-1-cyclohexen-2-yl)-3-(4-bromophenyl)-2-cyanopropanecarbothioamide

: 131270-67-2
hexamethyleneammonium 2-<1-(4-bromophenyl)-2-thiocarbamoyl-2-cyanoethyl>-5,5-dimethyl-3-oxo-1-cyclohexen-1-olate

Guidance literature:: Multi-step reaction with 3 steps

1: 1) morpholine, 2) aq. 10percent HCl / 1) C₂H₅OH, reflux, 3 h

2: 30 percent / KOH / dimethylformamide / 0.5 h / 25 °C

3: 80 percent / ethanol / 6 h / 25 °C

With morpholine; hydrogenchloride; potassium hydroxide; In ethanol; N,N-dimethyl-formamide;