6-(3,5-didecyloxyphenoxy)hexanoic acid N-(4-methoxycarbonylbenzyl)-N-(3-methoxycarbonylphenyl)amide

Base Information

Chemical Name:6-(3,5-didecyloxyphenoxy)hexanoic acid N-(4-methoxycarbonylbenzyl)-N-(3-methoxycarbonylphenyl)amide
CAS No.:912806-36-1
Molecular Formula:C₄₉H₇₁NO₈
Molecular Weight:802.105
Hs Code.:

Synonyms:6-(3,5-didecyloxyphenoxy)hexanoic acid N-(4-methoxycarbonylbenzyl)-N-(3-methoxycarbonylphenyl)amide

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Chemical Property of 6-(3,5-didecyloxyphenoxy)hexanoic acid N-(4-methoxycarbonylbenzyl)-N-(3-methoxycarbonylphenyl)amide

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Technology Process of 6-(3,5-didecyloxyphenoxy)hexanoic acid N-(4-methoxycarbonylbenzyl)-N-(3-methoxycarbonylphenyl)amide

There total 7 articles about 6-(3,5-didecyloxyphenoxy)hexanoic acid N-(4-methoxycarbonylbenzyl)-N-(3-methoxycarbonylphenyl)amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 912806-32-7
6-bromohexanoic acid N-(4-methoxycarbonylbenzyl)-N-(3-methoxycarbonylphenyl)amide

: 875210-88-1
3,5-didecyloxyphenol

: 912806-36-1
6-(3,5-didecyloxyphenoxy)hexanoic acid N-(4-methoxycarbonylbenzyl)-N-(3-methoxycarbonylphenyl)amide

Guidance literature:: With potassium carbonate; potassium iodide; In cyclohexanone; for 5h; Heating;
DOI:10.1021/jm060468y

Reference yield:

: 912806-29-2
C₁₇H₁₅NO₄

: 912806-36-1
6-(3,5-didecyloxyphenoxy)hexanoic acid N-(4-methoxycarbonylbenzyl)-N-(3-methoxycarbonylphenyl)amide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 88 percent / NaBH₄ / methanol / 24 h / 20 °C

2.1: sodium hydride / dibutyl ether / 2 h / 20 °C

2.2: 97 percent / dibutyl ether / 4 h / Heating

3.1: 83 percent / potassium carbonate; potassium iodide / cyclohexanone / 5 h / Heating

With sodium tetrahydroborate; sodium hydride; potassium carbonate; potassium iodide; In methanol; dibutyl ether; cyclohexanone;
DOI:10.1021/jm060468y

Reference yield:

: 912806-28-1
N-(4-methoxycarbonylbenzyl)-N-(3-methoxycarbonylphenyl)amine

: 912806-36-1
6-(3,5-didecyloxyphenoxy)hexanoic acid N-(4-methoxycarbonylbenzyl)-N-(3-methoxycarbonylphenyl)amide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / dibutyl ether / 2 h / 20 °C

1.2: 97 percent / dibutyl ether / 4 h / Heating

2.1: 83 percent / potassium carbonate; potassium iodide / cyclohexanone / 5 h / Heating

With sodium hydride; potassium carbonate; potassium iodide; In dibutyl ether; cyclohexanone;
DOI:10.1021/jm060468y