12-(trityloxy)-1-dodecanal

Base Information

Chemical Name:12-(trityloxy)-1-dodecanal
CAS No.:292820-10-1
Molecular Formula:C₃₁H₃₈O₂
Molecular Weight:442.642
Hs Code.:

Synonyms:12-(trityloxy)-1-dodecanal

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Chemical Property of 12-(trityloxy)-1-dodecanal

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Technology Process of 12-(trityloxy)-1-dodecanal

There total 6 articles about 12-(trityloxy)-1-dodecanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 889105-72-0
(((12,12-dimethoxydodecyl)oxy)methanetriyl)tribenzene

: 292820-10-1
12-(trityloxy)-1-dodecanal

Guidance literature:: (((12,12-dimethoxydodecyl)oxy)methanetriyl)tribenzene; With 2,6-dimethylpyridine; triethylsilyl trifluoromethyl sulfonate; In dichloromethane; at 0 ℃;

With water; In dichloromethane;
DOI:10.1021/ja060328d

Reference yield: 85.0%

: 158037-38-8
12-(trityloxy)-1-dodecanol

: 292820-10-1
12-(trityloxy)-1-dodecanal

Guidance literature:: 12-(trityloxy)-1-dodecanol; With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -78 ℃; for 0.333333h;

With triethylamine; In dichloromethane; at -78 - 20 ℃; for 1h;
DOI:10.1111/cbdd.12594

Reference yield:

: 5675-51-4
1,12-dodecandiol

: 292820-10-1
12-(trityloxy)-1-dodecanal

Guidance literature:: Multi-step reaction with 4 steps

1.1: 18 percent / PCC; Celite / CH₂Cl₂ / 1 h / 20 °C

2.1: 91 percent / p-TsOH / 20 °C

3.1: 83 percent / pyridine / CH₂Cl₂ / 3 h / 20 °C

4.1: TESOTf; 2,6-lutidine / CH₂Cl₂ / 0 °C

4.2: 92 percent / water / CH₂Cl₂

With pyridine; 2,6-dimethylpyridine; Celite; triethylsilyl trifluoromethyl sulfonate; toluene-4-sulfonic acid; pyridinium chlorochromate; In dichloromethane;
DOI:10.1021/ja060328d