1-(4'-bromophenyl)-6,7-dimethoxyisochroman

Base Information

Chemical Name:1-(4'-bromophenyl)-6,7-dimethoxyisochroman
CAS No.:187940-01-8
Molecular Formula:C₁₇H₁₇BrO₃
Molecular Weight:349.224
Hs Code.:

Synonyms:1-(4'-bromophenyl)-6,7-dimethoxyisochroman

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Chemical Property of 1-(4'-bromophenyl)-6,7-dimethoxyisochroman

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Technology Process of 1-(4'-bromophenyl)-6,7-dimethoxyisochroman

There total 1 articles about 1-(4'-bromophenyl)-6,7-dimethoxyisochroman which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1122-91-4
4-bromo-benzaldehyde

: 7417-21-2
2-(3,4-dimethoxyphenyl)ethyl alcohol

: 187940-01-8
1-(4'-bromophenyl)-6,7-dimethoxyisochroman

Guidance literature:: With silica-supported policresulen; at 80 ℃; for 3h; Green chemistry;
DOI:10.1016/S1872-2067(15)60910-X

Reference yield: 72.0%

: 187940-01-8
1-(4'-bromophenyl)-6,7-dimethoxyisochroman

: 187940-03-0
[2-(4-Bromo-benzoyl)-4,5-dimethoxy-phenyl]-acetic acid

Guidance literature:: With chromium(VI) oxide; sulfuric acid; In acetone; for 2h;
DOI:10.1021/jm960506l

Reference yield:

: 187940-01-8
1-(4'-bromophenyl)-6,7-dimethoxyisochroman

: 187940-09-6
1-(4-Bromo-phenyl)-7,8-dimethoxy-3,5-dihydro-benzo[d][1,2]diazepin-4-one

Guidance literature:: Multi-step reaction with 2 steps

1: CrO₃; H₂SO₄ / acetone; H₂O / 5 °C

2: NH₂NH₂*H₂O / ethanol / Heating

With chromium(VI) oxide; sulfuric acid; hydrazine hydrate; In ethanol; water; acetone;
DOI:10.1016/S0014-827X(01)01186-7