phenyl 2-O-benzoyl-3-O-benzyl-6-O-(p-methoxybenzyl)-1-thio-α-L-idopyranoside

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Chemical Name:phenyl 2-O-benzoyl-3-O-benzyl-6-O-(p-methoxybenzyl)-1-thio-α-L-idopyranoside
CAS No.:1447801-81-1
Molecular Formula:C₃₄H₃₄O₇S
Molecular Weight:586.706
Hs Code.:

Synonyms:phenyl 2-O-benzoyl-3-O-benzyl-6-O-(p-methoxybenzyl)-1-thio-α-L-idopyranoside

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Chemical Property of phenyl 2-O-benzoyl-3-O-benzyl-6-O-(p-methoxybenzyl)-1-thio-α-L-idopyranoside

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Technology Process of phenyl 2-O-benzoyl-3-O-benzyl-6-O-(p-methoxybenzyl)-1-thio-α-L-idopyranoside

There total 4 articles about phenyl 2-O-benzoyl-3-O-benzyl-6-O-(p-methoxybenzyl)-1-thio-α-L-idopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 1447801-79-7
phenyl 2-O-benzoyl-3-O-benzyl-4,6-O-(p-methoxybenzylidene)-1-thio-α-L-idopyranoside

: 1447801-81-1
phenyl 2-O-benzoyl-3-O-benzyl-6-O-(p-methoxybenzyl)-1-thio-α-L-idopyranoside

Guidance literature:: phenyl 2-O-benzoyl-3-O-benzyl-4,6-O-(p-methoxybenzylidene)-1-thio-α-L-idopyranoside; With iodine; for 0.0833333h; Inert atmosphere;

With sodium cyanoborohydride; In dichloromethane; at -20 ℃; for 0.25h; Inert atmosphere;
DOI:10.1021/jo400467g

Reference yield:

: C₂₁H₂₂O₆

: 1447801-81-1
phenyl 2-O-benzoyl-3-O-benzyl-6-O-(p-methoxybenzyl)-1-thio-α-L-idopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: zinc(II) iodide / dichloromethane / 20 °C

2.1: CSA / toluene / 2 h / Reflux

3.1: iodine / 0.08 h / Inert atmosphere

3.2: 0.25 h / -20 °C / Inert atmosphere

With iodine; zinc(II) iodide; In dichloromethane; toluene;
DOI:10.1021/jo400467g

Reference yield:

: 4551-15-9
phenylthiotrimethylsilane

: 1447801-81-1
phenyl 2-O-benzoyl-3-O-benzyl-6-O-(p-methoxybenzyl)-1-thio-α-L-idopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: zinc(II) iodide / dichloromethane / 20 °C

2.1: CSA / toluene / 2 h / Reflux

3.1: iodine / 0.08 h / Inert atmosphere

3.2: 0.25 h / -20 °C / Inert atmosphere

With iodine; zinc(II) iodide; In dichloromethane; toluene;
DOI:10.1021/jo400467g