dibenzyl (2S,3R)-5-hydroxycarbamoyl-2,2-dimethyl-[1,3]dioxolan-4-ylmethyl phosphate

Base Information

Chemical Name:dibenzyl (2S,3R)-5-hydroxycarbamoyl-2,2-dimethyl-[1,3]dioxolan-4-ylmethyl phosphate
CAS No.:870279-42-8
Molecular Formula:C₂₁H₂₆NO₈P
Molecular Weight:451.413
Hs Code.:

Synonyms:dibenzyl (2S,3R)-5-hydroxycarbamoyl-2,2-dimethyl-[1,3]dioxolan-4-ylmethyl phosphate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dibenzyl (2S,3R)-5-hydroxycarbamoyl-2,2-dimethyl-[1,3]dioxolan-4-ylmethyl phosphate

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Technology Process of dibenzyl (2S,3R)-5-hydroxycarbamoyl-2,2-dimethyl-[1,3]dioxolan-4-ylmethyl phosphate

There total 5 articles about dibenzyl (2S,3R)-5-hydroxycarbamoyl-2,2-dimethyl-[1,3]dioxolan-4-ylmethyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 798554-50-4
(2S,3R)-methyl 5-(bis-benzyloxyphosphoryloxymethyl)-2,2-dimethyl-[1,3]dioxolane-4-carboxylate

: 870279-42-8
dibenzyl (2S,3R)-5-hydroxycarbamoyl-2,2-dimethyl-[1,3]dioxolan-4-ylmethyl phosphate

Guidance literature:: With hydroxylamine hydrochloride; sodium methylate; In methanol; for 16h;
DOI:10.1021/jo0516786

Reference yield:

: 28762-00-7
(4S,5R)-methyl 5-(hydroxymethyl)-2,2-dimethyl-1,3-dioxolane-4-carboxylate

: 870279-42-8
dibenzyl (2S,3R)-5-hydroxycarbamoyl-2,2-dimethyl-[1,3]dioxolan-4-ylmethyl phosphate

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / pyridine / CH₂Cl₂ / 4 h / -30 - 20 °C

2: 80 percent / hydroxylamine hydrochloride; sodium methoxide / methanol / 16 h

With pyridine; hydroxylamine hydrochloride; sodium methylate; In methanol; dichloromethane;
DOI:10.1021/jo0516786

Reference yield:

: 15205-57-9
tribenzyl phosphite

: 870279-42-8
dibenzyl (2S,3R)-5-hydroxycarbamoyl-2,2-dimethyl-[1,3]dioxolan-4-ylmethyl phosphate

Guidance literature:: Multi-step reaction with 3 steps

1: I₂ / CH₂Cl₂ / -30 °C

2: 79 percent / pyridine / CH₂Cl₂ / 4 h / -30 - 20 °C

3: 80 percent / hydroxylamine hydrochloride; sodium methoxide / methanol / 16 h

With pyridine; hydroxylamine hydrochloride; iodine; sodium methylate; In methanol; dichloromethane;
DOI:10.1021/jo0516786