1-D-myo-inosityl-2-(N-acetyl-L-cysteinyl)amino-2-deoxy-α-D-glucopyranoside disulfide

Base Information

Chemical Name:1-D-myo-inosityl-2-(N-acetyl-L-cysteinyl)amino-2-deoxy-α-D-glucopyranoside disulfide
CAS No.:669091-43-4
Molecular Formula:C₃₄H₅₈N₄O₂₄S₂
Molecular Weight:970.979
Hs Code.:

Synonyms:1-D-myo-inosityl-2-(N-acetyl-L-cysteinyl)amino-2-deoxy-α-D-glucopyranoside disulfide

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Chemical Property of 1-D-myo-inosityl-2-(N-acetyl-L-cysteinyl)amino-2-deoxy-α-D-glucopyranoside disulfide

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Technology Process of 1-D-myo-inosityl-2-(N-acetyl-L-cysteinyl)amino-2-deoxy-α-D-glucopyranoside disulfide

There total 4 articles about 1-D-myo-inosityl-2-(N-acetyl-L-cysteinyl)amino-2-deoxy-α-D-glucopyranoside disulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 668481-15-0
Acetic acid (1S,2R,3R,4S,5S,6R)-2,3,4,5-tetraacetoxy-6-[(2R,3R,4R,5S,6R)-4,5-diacetoxy-6-acetoxymethyl-3-((R)-2-acetylamino-3-acetylsulfanyl-propionylamino)-tetrahydro-pyran-2-yloxy]-cyclohexyl ester

: 669091-43-4
1-D-myo-inosityl-2-(N-acetyl-L-cysteinyl)amino-2-deoxy-α-D-glucopyranoside disulfide

: 192126-76-4
1-O-(2'-[N-acetyl-L-cysteinyl]amido-2'-deoxy-α-D-glucopyranosyl)-D-myo-inositol

Guidance literature:: With magnesium methanolate; In methanol; at 20 ℃; for 2h;
DOI:10.1021/ol0362008

Reference yield:

: 668481-13-8
Acetic acid (1S,2R,3R,4S,5S,6R)-2,3,4,5-tetraacetoxy-6-((2R,3R,4R,5S,6R)-4,5-diacetoxy-6-acetoxymethyl-3-azido-tetrahydro-pyran-2-yloxy)-cyclohexyl ester

: 669091-43-4
1-D-myo-inosityl-2-(N-acetyl-L-cysteinyl)amino-2-deoxy-α-D-glucopyranoside disulfide

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / hydrogen; HCl / palladium on carbon / ethyl acetate / 6 h / 20 °C / 760.21 Torr

2: 1,3-dicyclohexylcarbodiimide

3: 29 percent / Mg(OMe)2 / methanol / 2 h / 20 °C

With hydrogenchloride; hydrogen; magnesium methanolate; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; ethyl acetate;
DOI:10.1021/ol0362008

Reference yield:

: 18725-37-6
(R)-2-acetylamino-3-(acetylthio)propionic acid

: 669091-43-4
1-D-myo-inosityl-2-(N-acetyl-L-cysteinyl)amino-2-deoxy-α-D-glucopyranoside disulfide

Guidance literature:: Multi-step reaction with 2 steps

1: 1,3-dicyclohexylcarbodiimide

2: 29 percent / Mg(OMe)2 / methanol / 2 h / 20 °C

With magnesium methanolate; dicyclohexyl-carbodiimide; In methanol;
DOI:10.1021/ol0362008