Technology Process of C31H42F3N3O5Si
There total 2 articles about C31H42F3N3O5Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: bromine / acetic acid
2: thionyl chloride; N,N-dimethyl-formamide / toluene
3: triethylamine / tetrahydrofuran
4: tetrahydrofuran
5: potassium carbonate / N,N-dimethyl-formamide
6: 1H-imidazole / N,N-dimethyl-formamide
7: palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / 1,4-dioxane
With
1H-imidazole; thionyl chloride; bromine; palladium diacetate; potassium carbonate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triethylamine; N,N-dimethyl-formamide;
In
tetrahydrofuran; 1,4-dioxane; acetic acid; N,N-dimethyl-formamide; toluene;
7: Buchwald coupling;
DOI:10.1016/j.bmcl.2010.11.108
- Guidance literature:
-
With
palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl;
In
1,4-dioxane;
DOI:10.1016/j.bmcl.2010.11.108