(1S,2S,7S,8aR)-2-(benzoyloxy)-7-hydroxyoctahydro-1-indolizinyl benzoate

Base Information

• Chemical Name: (1S,2S,7S,8aR)-2-(benzoyloxy)-7-hydroxyoctahydro-1-indolizinyl benzoate
• CAS No.: 1350293-84-3
• Molecular Formula: C₂₂H₂₃NO₅
• Molecular Weight: 381.428

Synonyms:(1S,2S,7S,8aR)-2-(benzoyloxy)-7-hydroxyoctahydro-1-indolizinyl benzoate

Chemical Property of (1S,2S,7S,8aR)-2-(benzoyloxy)-7-hydroxyoctahydro-1-indolizinyl benzoate

Chemical Property:

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Technology Process of (1S,2S,7S,8aR)-2-(benzoyloxy)-7-hydroxyoctahydro-1-indolizinyl benzoate

There total 2 articles about (1S,2S,7S,8aR)-2-(benzoyloxy)-7-hydroxyoctahydro-1-indolizinyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C23H25NO8S → (1S,2S,7R,8aS)-2-(benzoyloxy)-7-hydroxyoctahydro-1-indolizinyl benzoate (1192356-86-7) + (1S,2S,7S,8aR)-2-(benzoyloxy)-7-hydroxyoctahydro-1-indolizinyl benzoate (1350293-84-3)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In methanol; under 760.051 Torr;

DOI:10.1016/j.tet.2011.10.008

Reference yield:

(4S,5S)-5-(benzoyloxy)-2-(2-hydroxyethyl)hexahydropyrrolo[1,2-b]isoxazol-4-yl benzoate → (1S,2S,7R,8aS)-2-(benzoyloxy)-7-hydroxyoctahydro-1-indolizinyl benzoate (1192356-86-7) + (1S,2S,7S,8aR)-2-(benzoyloxy)-7-hydroxyoctahydro-1-indolizinyl benzoate (1350293-84-3)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 1 h / 0 °C / Inert atmosphere

2: palladium 10% on activated carbon; hydrogen / methanol / 760.05 Torr

With palladium 10% on activated carbon; hydrogen; triethylamine; In methanol; dichloromethane;

DOI:10.1016/j.tet.2011.10.008

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