Technology Process of C22H25NO4
There total 7 articles about C22H25NO4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C22H23NO5;
With
borane-THF;
In
tetrahydrofuran;
at 0 ℃;
for 1h;
Inert atmosphere;
With
hydrogenchloride;
In
methanol; water;
at 20 ℃;
for 1h;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: palladium 10% on activated carbon; hydrogen / methanol / 20 °C / 760.05 Torr
2.1: borane-THF / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere
2.2: 1 h / 20 °C
With
borane-THF; palladium 10% on activated carbon; hydrogen;
In
tetrahydrofuran; methanol;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: thionyl chloride / 7 h / Reflux
2.1: thionyl chloride / 0.5 h / Reflux
2.2: 2 h / 0 - 20 °C
3.1: Jones reagent / acetone / 0.33 h / 0 - 20 °C
4.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C
4.2: 0.67 h / 0 °C
5.1: palladium 10% on activated carbon; hydrogen / methanol / 20 °C / 760.05 Torr
6.1: borane-THF / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere
6.2: 1 h / 20 °C
With
thionyl chloride; borane-THF; palladium 10% on activated carbon; Jones reagent; hydrogen; sodium hydride;
In
tetrahydrofuran; methanol; acetone; mineral oil;