4-<<2-(1H-imidazol-1-yl)-1-<<(4-methoxyphenyl)methoxy>methyl>ethoxy>methyl>-N,N-dimethylbenzenecarbothioamide

Base Information

Chemical Name:4-<<2-(1H-imidazol-1-yl)-1-<<(4-methoxyphenyl)methoxy>methyl>ethoxy>methyl>-N,N-dimethylbenzenecarbothioamide
CAS No.:108836-61-9
Molecular Formula:C₂₄H₂₉N₃O₃S
Molecular Weight:439.579
Hs Code.:

Synonyms:4-<<2-(1H-imidazol-1-yl)-1-<<(4-methoxyphenyl)methoxy>methyl>ethoxy>methyl>-N,N-dimethylbenzenecarbothioamide

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Chemical Property of 4-<<2-(1H-imidazol-1-yl)-1-<<(4-methoxyphenyl)methoxy>methyl>ethoxy>methyl>-N,N-dimethylbenzenecarbothioamide

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Technology Process of 4-<<2-(1H-imidazol-1-yl)-1-<<(4-methoxyphenyl)methoxy>methyl>ethoxy>methyl>-N,N-dimethylbenzenecarbothioamide

There total 7 articles about 4-<<2-(1H-imidazol-1-yl)-1-<<(4-methoxyphenyl)methoxy>methyl>ethoxy>methyl>-N,N-dimethylbenzenecarbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 108836-59-5
4-[2-Imidazol-1-yl-1-(4-methoxy-benzyloxymethyl)-ethoxymethyl]-N,N-dimethyl-benzamide

: 108836-61-9
4-<<2-(1H-imidazol-1-yl)-1-<<(4-methoxyphenyl)methoxy>methyl>ethoxy>methyl>-N,N-dimethylbenzenecarbothioamide

Guidance literature:: With Lawessons reagent; In benzene; for 5h; Heating;
DOI:10.1021/jm00392a011

Reference yield:

: 108836-41-5
2-((4-methoxybenzyloxy)methyl)oxirane

: 108836-61-9
4-<<2-(1H-imidazol-1-yl)-1-<<(4-methoxyphenyl)methoxy>methyl>ethoxy>methyl>-N,N-dimethylbenzenecarbothioamide

Guidance literature:: Multi-step reaction with 6 steps

1: 61 percent / tetrahydrofuran / 16 h / Heating

2: 1.) NaH / 1.) THF, RT, 1 h, 2.) THF, 16 h

3: 80 percent / 10percent ethanolic KOH / 24 h / 18 °C

4: Et₃N / CH₂Cl₂ / 0.5 h / 0 °C

5: CH₂Cl₂ / 2 h / Ambient temperature

6: 48 percent / 2,4-bis(4-methoxyphenyl)-1,3,2,4-dithiadiphosphetane 2,4-disulfide / benzene / 5 h / Heating

With Lawessons reagent; potassium hydroxide; sodium hydride; triethylamine; In tetrahydrofuran; dichloromethane; benzene;
DOI:10.1021/jm00392a011

Reference yield:

: 84727-35-5
1-[2-hydroxy-3-[(4-methoxyphenyl)methoxy]propyl]-1H-imidazole

: 108836-61-9
4-<<2-(1H-imidazol-1-yl)-1-<<(4-methoxyphenyl)methoxy>methyl>ethoxy>methyl>-N,N-dimethylbenzenecarbothioamide

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) NaH / 1.) THF, RT, 1 h, 2.) THF, 16 h

2: 80 percent / 10percent ethanolic KOH / 24 h / 18 °C

3: Et₃N / CH₂Cl₂ / 0.5 h / 0 °C

4: CH₂Cl₂ / 2 h / Ambient temperature

5: 48 percent / 2,4-bis(4-methoxyphenyl)-1,3,2,4-dithiadiphosphetane 2,4-disulfide / benzene / 5 h / Heating

With Lawessons reagent; potassium hydroxide; sodium hydride; triethylamine; In dichloromethane; benzene;
DOI:10.1021/jm00392a011