(Z)-S-1-(4-methoxyphenyl)-3-oxoprop-1-en-2-yl diisopropylcarbamothioate

Base Information

Chemical Name:(Z)-S-1-(4-methoxyphenyl)-3-oxoprop-1-en-2-yl diisopropylcarbamothioate
CAS No.:1379480-17-7
Molecular Formula:C₁₇H₂₃NO₃S
Molecular Weight:321.441
Hs Code.:

Synonyms:(Z)-S-1-(4-methoxyphenyl)-3-oxoprop-1-en-2-yl diisopropylcarbamothioate

Suppliers and Price of (Z)-S-1-(4-methoxyphenyl)-3-oxoprop-1-en-2-yl diisopropylcarbamothioate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-S-1-(4-methoxyphenyl)-3-oxoprop-1-en-2-yl diisopropylcarbamothioate

Chemical Property:

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Technology Process of (Z)-S-1-(4-methoxyphenyl)-3-oxoprop-1-en-2-yl diisopropylcarbamothioate

There total 6 articles about (Z)-S-1-(4-methoxyphenyl)-3-oxoprop-1-en-2-yl diisopropylcarbamothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₁H₃₃NO₄S

: 1379480-17-7
(Z)-S-1-(4-methoxyphenyl)-3-oxoprop-1-en-2-yl diisopropylcarbamothioate

Guidance literature:: With formic acid; In dichloromethane; at 20 ℃; for 72h;
DOI:10.1021/ol300921f

Reference yield:

: 1379480-20-2
(Z)-1-(2-bromo-3,3-diethoxyprop-1-enyl)-4-methoxybenzene

: 1379480-17-7
(Z)-S-1-(4-methoxyphenyl)-3-oxoprop-1-en-2-yl diisopropylcarbamothioate

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / -78 °C

1.2: 1 h / -78 °C

2.1: formic acid / dichloromethane / 72 h / 20 °C

With n-butyllithium; formic acid; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1021/ol300921f

Reference yield:

: 108-18-9
diisopropylamine

: 1379480-17-7
(Z)-S-1-(4-methoxyphenyl)-3-oxoprop-1-en-2-yl diisopropylcarbamothioate

Guidance literature:: Multi-step reaction with 3 steps

1.1: dichloromethane / 1 h / 0 - 20 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / -78 °C

2.2: 1 h / -78 °C

3.1: formic acid / dichloromethane / 72 h / 20 °C

With n-butyllithium; formic acid; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1021/ol300921f