4-chlorobenzyl hydrazinecarboxylate

Base Information

• Chemical Name: 4-chlorobenzyl hydrazinecarboxylate
• CAS No.: 3057-24-7
• Molecular Formula: C₈H₉ClN₂O₂
• Molecular Weight: 200.625
• Mol file: 3057-24-7.mol

Synonyms:4-chlorobenzyl hydrazinecarboxylate

Chemical Property of 4-chlorobenzyl hydrazinecarboxylate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-chlorobenzyl hydrazinecarboxylate

There total 3 articles about 4-chlorobenzyl hydrazinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

imidazole-1-carboxylic acid 4-chloro-benzyl ester → 4-chlorobenzyl hydrazinecarboxylate (3057-24-7)

Guidance literature:

With hydrazine hydrate; In dichloromethane; at 0 - 20 ℃; for 1.5h;

DOI:10.1016/j.tet.2017.07.033

Reference yield:

para-Chlorobenzyl alcohol (873-76-7) → 4-chlorobenzyl hydrazinecarboxylate (3057-24-7)

Guidance literature:

Multi-step reaction with 2 steps

1: dichloromethane / 1 h / 20 °C

2: hydrazine hydrate / dichloromethane / 1.5 h / 0 - 20 °C

With hydrazine hydrate; In dichloromethane;

DOI:10.1016/j.tet.2017.07.033

Reference yield:

→ 4-chlorobenzyl hydrazinecarboxylate (3057-24-7)

Guidance literature:

upstream raw materials:

para-Chlorobenzyl alcohol