methyl 4-(methylsulfanyl)dithiobenzoate

Base Information

• Chemical Name: methyl 4-(methylsulfanyl)dithiobenzoate
• CAS No.: 5969-48-2
• Molecular Formula: C₉H₁₀S₃
• Molecular Weight: 214.376
• Mol file: 5969-48-2.mol

Synonyms:methyl 4-(methylsulfanyl)dithiobenzoate

Chemical Property of methyl 4-(methylsulfanyl)dithiobenzoate

Chemical Property:

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of methyl 4-(methylsulfanyl)dithiobenzoate

There total 1 articles about methyl 4-(methylsulfanyl)dithiobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Sodium; 4-methylsulfanyl-dithiobenzoate + dimethyl sulfate (77-78-1) → methyl 4-(methylsulfanyl)dithiobenzoate (5969-48-2)

Guidance literature:

Reference yield: 86.0%

methyl 4-(methylsulfanyl)dithiobenzoate (5969-48-2) → 4-(methylthio)benzoic acid (13205-48-6,562836-64-0)

Guidance literature:

With sodium hydroxide; dihydrogen peroxide; In methanol; water; at 20 ℃; for 0.0833333h;

DOI:10.1055/s-0028-1083190

Reference yield: 78.0%

2-Acetylthiazole (24295-03-2,260998-74-1) + methyl 4-(methylsulfanyl)dithiobenzoate (5969-48-2) → C13H11NOS3

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃;

DOI:10.1021/acs.joc.0c02216

upstream raw materials:

dimethyl sulfate

Downstream raw materials:

4-(methylthio)benzoic acid