p-methoxybenzyl 6-(N-nitroso)-acetamido-2-azido-2,6-dideoxy-3,4-O-isopropylidene-α-D-galactopyranoside

Base Information

Chemical Name:p-methoxybenzyl 6-(N-nitroso)-acetamido-2-azido-2,6-dideoxy-3,4-O-isopropylidene-α-D-galactopyranoside
CAS No.:664998-01-0
Molecular Formula:C₁₉H₂₅N₅O₇
Molecular Weight:435.437
Hs Code.:

Synonyms:p-methoxybenzyl 6-(N-nitroso)-acetamido-2-azido-2,6-dideoxy-3,4-O-isopropylidene-α-D-galactopyranoside

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Chemical Property of p-methoxybenzyl 6-(N-nitroso)-acetamido-2-azido-2,6-dideoxy-3,4-O-isopropylidene-α-D-galactopyranoside

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Technology Process of p-methoxybenzyl 6-(N-nitroso)-acetamido-2-azido-2,6-dideoxy-3,4-O-isopropylidene-α-D-galactopyranoside

There total 6 articles about p-methoxybenzyl 6-(N-nitroso)-acetamido-2-azido-2,6-dideoxy-3,4-O-isopropylidene-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 664998-00-9
p-methoxybenzyl 6-acetamido-2-azido-2,6-dideoxy-3,4-O-isopropylidene-α-D-galactopyranoside

: 664998-01-0
p-methoxybenzyl 6-(N-nitroso)-acetamido-2-azido-2,6-dideoxy-3,4-O-isopropylidene-α-D-galactopyranoside

Guidance literature:: With acetic anhydride; acetic acid; sodium nitrite; at -10 ℃; for 1h;
DOI:10.1039/b307674a

Reference yield:

: 664997-97-1
p-methoxybenzyl 2-azido-2-deoxy-3,4-O-isopropylidene-α-D-galactopyranoside

: 664998-01-0
p-methoxybenzyl 6-(N-nitroso)-acetamido-2-azido-2,6-dideoxy-3,4-O-isopropylidene-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 88 percent / pyridine / 8.25 h / 0 - 25 °C

2: 99 percent / dimethylformamide / 48 h / Heating

3: NH₂NH₂ / methanol; tetrahydrofuran / 12 h / 25 °C

4: 74 mg / pyridine / 1.5 h / 0 - 25 °C

5: 82 percent / NaNO₂; Ac₂O; AcOH / 1 h / -10 °C

With pyridine; acetic anhydride; acetic acid; hydrazine; sodium nitrite; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1039/b307674a

Reference yield:

: 664997-98-2
p-methoxybenzyl 2-azido-2-deoxy-3,4-O-isopropylidene-6-p-toluenesulfonyl-α-D-galactopyranoside

: 664998-01-0
p-methoxybenzyl 6-(N-nitroso)-acetamido-2-azido-2,6-dideoxy-3,4-O-isopropylidene-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / dimethylformamide / 48 h / Heating

2: NH₂NH₂ / methanol; tetrahydrofuran / 12 h / 25 °C

3: 74 mg / pyridine / 1.5 h / 0 - 25 °C

4: 82 percent / NaNO₂; Ac₂O; AcOH / 1 h / -10 °C

With pyridine; acetic anhydride; acetic acid; hydrazine; sodium nitrite; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1039/b307674a