2-N-phenoxyacetyl-6-(3-O-L-menthylpropenyl)-9-(5'-O-[4,4'-dimethoxytrityl]-2'-deoxy-β-D-ribofuranosyl)purine

Base Information

• Chemical Name: 2-N-phenoxyacetyl-6-(3-O-L-menthylpropenyl)-9-(5'-O-[4,4'-dimethoxytrityl]-2'-deoxy-β-D-ribofuranosyl)purine
• CAS No.: 1204045-51-1
• Molecular Formula: C₅₂H₅₉N₅O₈
• Molecular Weight: 882.069

Synonyms:2-N-phenoxyacetyl-6-(3-O-L-menthylpropenyl)-9-(5'-O-[4,4'-dimethoxytrityl]-2'-deoxy-β-D-ribofuranosyl)purine

Chemical Property of 2-N-phenoxyacetyl-6-(3-O-L-menthylpropenyl)-9-(5'-O-[4,4'-dimethoxytrityl]-2'-deoxy-β-D-ribofuranosyl)purine

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Technology Process of 2-N-phenoxyacetyl-6-(3-O-L-menthylpropenyl)-9-(5'-O-[4,4'-dimethoxytrityl]-2'-deoxy-β-D-ribofuranosyl)purine

There total 1 articles about 2-N-phenoxyacetyl-6-(3-O-L-menthylpropenyl)-9-(5'-O-[4,4'-dimethoxytrityl]-2'-deoxy-β-D-ribofuranosyl)purine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

2-N-phenoxyacetyl-6-(3-O-L-menthylpropenyl)-9-(2'-deoxy-β-D-ribofuranosyl)purine (1204045-50-0) + 4,4'-dimethoxytrityl chloride (40615-36-9) → 2-N-phenoxyacetyl-6-(3-O-L-menthylpropenyl)-9-(5'-O-[4,4'-dimethoxytrityl]-2'-deoxy-β-D-ribofuranosyl)purine (1204045-51-1)

Guidance literature:

With triethylamine; In dichloromethane; at 0 ℃; regioselective reaction; Inert atmosphere;

DOI:10.1016/j.tet.2009.10.023

Reference yield: 84.0%

2-N-phenoxyacetyl-6-(3-O-L-menthylpropenyl)-9-(5'-O-[4,4'-dimethoxytrityl]-2'-deoxy-β-D-ribofuranosyl)purine (1204045-51-1) + 2-cyanoethyl-N,N-(diisopropylamino)chlorophosphine (124482-92-4,89992-70-1) → 2-N-phenoxyacetyl-6-(3-O-L-menthylpropenyl)-9-(5'-O-[4,4'-dimethoxytrityl]-3'-O-[{N,N-diisopropylamino}-2-cyanoethoxyphosphite]-2'-deoxy-β-D-ribofuranosyl)purine (1204045-45-3)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 ℃; Inert atmosphere;

DOI:10.1016/j.tet.2009.10.023

upstream raw materials:

2-N-phenoxyacetyl-6-(3-O-L-menthylpropenyl)-9-(2'-deoxy-β-D-ribofuranosyl)purine

4,4'-dimethoxytrityl chloride

Downstream raw materials:

2-N-phenoxyacetyl-6-(3-O-L-menthylpropenyl)-9-(5'-O-[4,4'-dimethoxytrityl]-3'-O-[{N,N-diisopropylamino}-2-cyanoethoxyphosphite]-2'-deoxy-β-D-ribofuranosyl)purine

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