C₃₂H₄₄N₂O₄Si

Base Information

• Chemical Name: C₃₂H₄₄N₂O₄Si
• CAS No.: 130253-43-9
• Molecular Formula: C₃₂H₄₄N₂O₄Si
• Molecular Weight: 548.798
• Mol file: 130253-43-9.mol

Synonyms:C₃₂H₄₄N₂O₄Si

Chemical Property of C₃₂H₄₄N₂O₄Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₂H₄₄N₂O₄Si

There total 11 articles about C₃₂H₄₄N₂O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

C34H46N2O5Si (130278-18-1) → C32H44N2O4Si (130253-43-9)

Guidance literature:

With potassium hydroxide; In methanol;

DOI:10.1016/S0040-4039(00)88787-0

Reference yield:

C29H34N2O5 (130278-17-0) → C32H44N2O4Si (130253-43-9)

Guidance literature:

Multi-step reaction with 6 steps

1: 90 percent / CH₂Cl₂

2: 68 percent / Pb(OAc)4 / CH₂Cl₂ / -70 °C

3: AcOH / tetrahydrofuran; H₂O / Ambient temperature

4: 80 percent / NaBH₄ / methanol / 0 °C

5: 80 percent / Et₃N / CH₂Cl₂

6: 90 percent / aq. KOH / methanol

With lead(IV) acetate; potassium hydroxide; sodium tetrahydroborate; acetic acid; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water;

DOI:10.1016/S0040-4039(00)88787-0

Reference yield:

C28H30N2O5 → C32H44N2O4Si (130253-43-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 80 percent / NaBH₄ / methanol / 0 °C

2: 80 percent / Et₃N / CH₂Cl₂

3: 90 percent / aq. KOH / methanol

With potassium hydroxide; sodium tetrahydroborate; triethylamine; In methanol; dichloromethane;

DOI:10.1016/S0040-4039(00)88787-0

upstream raw materials:

C₃₄H₄₆N₂O₅Si

C₂₈H₃₂N₂O₅

C₂₉H₃₄N₂O₅

C₃₃H₄₄N₂O₄Si

Downstream raw materials:

C₂₆H₂₈N₂O₃

C₃₃H₄₆N₂O₆SSi