C₅₃H₇₈N₂O₇Si

Base Information

Chemical Name:C₅₃H₇₈N₂O₇Si
CAS No.:947412-61-5
Molecular Formula:C₅₃H₇₈N₂O₇Si
Molecular Weight:883.297
Hs Code.:

C<sub>53</sub>H<sub>78</sub>N<sub>2</sub>O<sub>7</sub>Si

Synonyms:C₅₃H₇₈N₂O₇Si

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Chemical Property of C₅₃H₇₈N₂O₇Si

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Technology Process of C₅₃H₇₈N₂O₇Si

There total 25 articles about C₅₃H₇₈N₂O₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₇H₅₅NO₄

: (2S)-2-benzamido-3-[tert-butyl(dimethyl)silyl]oxypropanoic acid

: 947412-61-5
C₅₃H₇₈N₂O₇Si

Guidance literature:: With 4-methyl-morpholine; benzotriazol-1-ol; In dichloromethane; at 0 - 20 ℃; for 20h;
DOI:10.1021/ja072334v

Reference yield:

: 947412-29-5
(2E,4E,6S,7S,8E)-1-(2-trimethylsilylethoxycarbonylamino)-9-iodo-2,5,7-trimethylnona-2,4,8-trien-6-ol

: 947412-61-5
C₅₃H₇₈N₂O₇Si

Guidance literature:: Multi-step reaction with 5 steps

1: 70 percent / Ba(OH)2*8H₂O / (dppf)PdCl₂ / dimethylformamide / 2 h / 20 °C

2: 78 percent / N-(3-dimethylaminopropyl)-N'-ethyl-carbodiimide*HCl; 4-pyrrolidino-pyridine / CH₂Cl₂ / 96 h / 20 °C

3: 78 percent / Grubbs second generation catalyst / CH₂Cl₂ / 72 h / 20 °C

4: TBAF / tetrahydrofuran / 36 h / 0 - 20 °C

5: 1-hydroxy-benzotriazole; N-methylmorpholine; N-3-(dimethylaminopropyl)-N'-ethyl-carbodiimide*HCl / CH₂Cl₂ / 20 h / 0 - 20 °C

With 4-methyl-morpholine; barium dihydroxide; tetrabutyl ammonium fluoride; benzotriazol-1-ol; 4-pyrrolidin-1-ylpyridine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 1: Suzuki reaction;
DOI:10.1021/ja072334v

Reference yield:

: 914374-92-8
(3S)-1-(trimethylsilyl)hept-6-en-1-yn-3-ol

: 947412-61-5
C₅₃H₇₈N₂O₇Si

Guidance literature:: Multi-step reaction with 13 steps

1.1: n-BuLi / hexane; tetrahydrofuran / 0.33 h / -78 °C

1.2: hexane; tetrahydrofuran; dimethylsulfoxide / -78 - 20 °C

2.1: 995 mg / 2,6-lutidine; NaIO₄; OsO₄ / dioxane; H₂O; 2-methyl-propan-2-ol / 3 h

3.1: 18-crown-6; KHMDS / toluene / 0.75 h / 0 °C

3.2: toluene / 1.92 h / -20 - 0 °C

4.1: DIBAl-H / hexane; CH₂Cl₂ / 1 h / -78 °C

5.1: MnO₂ / CH₂Cl₂ / 13 h / 20 °C

6.1: n-BuLi / hexane; tetrahydrofuran / 0.5 h / -78 - 20 °C

6.2: 243 mg / hexane; tetrahydrofuran / 1 h / -78 - 20 °C

7.1: 83 percent / K₂CO₃ / methanol / 3 h

8.1: 56 percent / 9-BBN / tetrahydrofuran / 60 h / 45 °C

9.1: 70 percent / Ba(OH)2*8H₂O / (dppf)PdCl₂ / dimethylformamide / 2 h / 20 °C

10.1: 78 percent / N-(3-dimethylaminopropyl)-N'-ethyl-carbodiimide*HCl; 4-pyrrolidino-pyridine / CH₂Cl₂ / 96 h / 20 °C

11.1: 78 percent / Grubbs second generation catalyst / CH₂Cl₂ / 72 h / 20 °C

12.1: TBAF / tetrahydrofuran / 36 h / 0 - 20 °C

13.1: 1-hydroxy-benzotriazole; N-methylmorpholine; N-3-(dimethylaminopropyl)-N'-ethyl-carbodiimide*HCl / CH₂Cl₂ / 20 h / 0 - 20 °C

With 4-methyl-morpholine; 2,6-dimethylpyridine; manganese(IV) oxide; barium dihydroxide; sodium periodate; osmium(VIII) oxide; n-butyllithium; 18-crown-6 ether; tetrabutyl ammonium fluoride; potassium hexamethylsilazane; diisobutylaluminium hydride; potassium carbonate; benzotriazol-1-ol; 4-pyrrolidin-1-ylpyridine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; 9-borabicyclo[3.3.1]nonane dimer; In tetrahydrofuran; 1,4-dioxane; methanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; toluene; tert-butyl alcohol; 3.1: Still-Gennari olefination / 3.2: Still-Gennari olefination / 6.2: Wittig olefination / 9.1: Suzuki reaction;
DOI:10.1021/ja072334v