2-chloro-4-sulfone

Base Information

Chemical Name:2-chloro-4-sulfone
CAS No.:1352310-98-5
Molecular Formula:C₂₅H₃₄ClNO₇S
Molecular Weight:528.066
Hs Code.:

Synonyms:2-chloro-4-sulfone

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Chemical Property of 2-chloro-4-sulfone

Chemical Property:

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Technology Process of 2-chloro-4-sulfone

There total 4 articles about 2-chloro-4-sulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 42986-91-4
2,4-di-(methylsulfonyl)-aniline

: 508234-34-2
3-(10-deoxoartemisin-10-yl)propanoic acid

: 1352310-98-5
2-chloro-4-sulfone

Guidance literature:: 3-(10-deoxoartemisin-10-yl)propanoic acid; With 4-methyl-morpholine; isobutyl chloroformate; In tetrahydrofuran; at -40 ℃; for 1h;

2,4-di-(methylsulfonyl)-aniline; With n-butyllithium; In tetrahydrofuran; toluene; at -78 - 0 ℃; for 0.5h;
DOI:10.1021/jm201214d

Reference yield:

: 142893-80-9
10-deoxoallylartemisinin

: 1352310-98-5
2-chloro-4-sulfone

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium perborate tetrahydrate; dimethyl sulfide borane

2.1: sodium periodate; ruthenium trichloride

3.1: 4-methyl-morpholine; isobutyl chloroformate / tetrahydrofuran / 1 h / -40 °C

3.2: 0.5 h / -78 - 0 °C

With 4-methyl-morpholine; ruthenium trichloride; sodium periodate; sodium perborate tetrahydrate; dimethyl sulfide borane; isobutyl chloroformate; In tetrahydrofuran;
DOI:10.1021/jm201214d

Reference yield:

: 75887-51-3
dihydroartemisinin acetate

: 1352310-98-5
2-chloro-4-sulfone

Guidance literature:: Multi-step reaction with 4 steps

1.1: tin(IV) chloride

2.1: sodium perborate tetrahydrate; dimethyl sulfide borane

3.1: sodium periodate; ruthenium trichloride

4.1: 4-methyl-morpholine; isobutyl chloroformate / tetrahydrofuran / 1 h / -40 °C

4.2: 0.5 h / -78 - 0 °C

With 4-methyl-morpholine; ruthenium trichloride; sodium periodate; sodium perborate tetrahydrate; dimethyl sulfide borane; tin(IV) chloride; isobutyl chloroformate; In tetrahydrofuran;
DOI:10.1021/jm201214d