(1S,3R)-3,5-bis(benzyloxy)-1-(2-iodoethyl)-2,2-dimethylpentyl propionate

Base Information

Chemical Name:(1S,3R)-3,5-bis(benzyloxy)-1-(2-iodoethyl)-2,2-dimethylpentyl propionate
CAS No.:115378-58-0
Molecular Formula:C₂₆H₃₅IO₄
Molecular Weight:538.466
Hs Code.:

Synonyms:(1S,3R)-3,5-bis(benzyloxy)-1-(2-iodoethyl)-2,2-dimethylpentyl propionate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,3R)-3,5-bis(benzyloxy)-1-(2-iodoethyl)-2,2-dimethylpentyl propionate

Chemical Property:

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Technology Process of (1S,3R)-3,5-bis(benzyloxy)-1-(2-iodoethyl)-2,2-dimethylpentyl propionate

There total 5 articles about (1S,3R)-3,5-bis(benzyloxy)-1-(2-iodoethyl)-2,2-dimethylpentyl propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 115378-57-9
Propionic acid (1S,3R)-3,5-bis-benzyloxy-2,2-dimethyl-1-[2-(toluene-4-sulfonyloxy)-ethyl]-pentyl ester

: 115378-58-0
(1S,3R)-3,5-bis(benzyloxy)-1-(2-iodoethyl)-2,2-dimethylpentyl propionate

Guidance literature:: With potassium iodide; In dimethyl sulfoxide; for 12h; Ambient temperature;
DOI:10.1016/S0040-4020(01)81517-9

Reference yield:

: 115378-52-4
(4S,6R)-6,8-bis(benzyloxy)-5,5-dimethyl-1-octen-4-ol

: 115378-58-0
(1S,3R)-3,5-bis(benzyloxy)-1-(2-iodoethyl)-2,2-dimethylpentyl propionate

Guidance literature:: Yield given. Multistep reaction;
DOI:10.1246/cl.1987.2097

Reference yield:

: 115378-54-6
Propionic acid (1S,3R)-1-allyl-3,5-bis-benzyloxy-2,2-dimethyl-pentyl ester

: 115378-58-0
(1S,3R)-3,5-bis(benzyloxy)-1-(2-iodoethyl)-2,2-dimethylpentyl propionate

Guidance literature:: Multi-step reaction with 4 steps

1: OsO₄, NaIO₄ / diethyl ether; H₂O / Ambient temperature

2: NaBH₄ / ethanol / 0 °C

3: DMAP, Et₃N / Ambient temperature

4: KI / dimethylsulfoxide / Ambient temperature

With dmap; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; triethylamine; potassium iodide; In diethyl ether; ethanol; water; dimethyl sulfoxide;
DOI:10.1246/cl.1987.2097