C₃₁H₅₂O₅Si₂

Base Information

Chemical Name:C₃₁H₅₂O₅Si₂
CAS No.:948837-54-5
Molecular Formula:C₃₁H₅₂O₅Si₂
Molecular Weight:560.922
Hs Code.:

C<sub>31</sub>H<sub>52</sub>O<sub>5</sub>Si<sub>2</sub>

Synonyms:C₃₁H₅₂O₅Si₂

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Chemical Property of C₃₁H₅₂O₅Si₂

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Technology Process of C₃₁H₅₂O₅Si₂

There total 20 articles about C₃₁H₅₂O₅Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₁H₅₂O₄Si₂

: 948837-54-5
C₃₁H₅₂O₅Si₂

Guidance literature:: With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; In tetrahydrofuran; water; tert-butyl alcohol; at 20 ℃;
DOI:10.1016/j.tetlet.2007.05.174

Reference yield:

: 59382-59-1
2-methyl-3-nitro-benzoic acid methyl ester

: 948837-54-5
C₃₁H₅₂O₅Si₂

Guidance literature:: Multi-step reaction with 14 steps

1.1: H₂ / Pd/C / ethanol / 20 °C

1.2: 78 percent / NaNO₂; H₂SO₄ / Heating

2.1: 83 percent / Br₂ / CH₂Cl₂ / -45 °C

3.1: 92 percent / imidazole / dimethylformamide / 20 °C

4.1: 95 percent / diisobutylaluminum hydride / CH₂Cl₂ / -78 °C

5.1: 90 percent / PPTS / CH₂Cl₂ / 20 °C

6.1: n-BuLi / tetrahydrofuran / -78 °C

7.1: NaH / tetrahydrofuran / 20 °C

8.1: 73 percent / CBr₄; PPh₃ / CH₂Cl₂ / 40 °C

9.1: t-BuLi / diethyl ether / -78 °C

9.2: PPh₃ / Pd₂(dba)3 / dimethylformamide / 30 °C

10.1: 85 percent / 1,3-propanedithiol; BF₃*OEt₂ / CH₂Cl₂ / -78 °C

11.1: imidazole / dimethylformamide / 0 °C

12.1: DIBALH / CH₂Cl₂ / -78 °C

13.1: MnO₂ / CH₂Cl₂ / 20 °C

14.1: NaClO₂; NaH₂PO₄; 2-methyl-2-butene / tetrahydrofuran; 2-methyl-propan-2-ol; H₂O / 20 °C

With 1H-imidazole; 1.3-propanedithiol; manganese(IV) oxide; sodium chlorite; sodium dihydrogenphosphate; n-butyllithium; 2-methyl-but-2-ene; carbon tetrabromide; boron trifluoride diethyl etherate; hydrogen; bromine; tert.-butyl lithium; pyridinium p-toluenesulfonate; sodium hydride; diisobutylaluminium hydride; triphenylphosphine; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol; 1.2: Sandmeyer reaction / 7.1: Horner-Wadsworth-Emmons reaction / 9.2: Stille reaction / 14.1: Pinnic oxidation;
DOI:10.1016/j.tetlet.2007.05.174

Reference yield:

: 1975-50-4
2-methyl-3-nitrobenzic acid

: 948837-54-5
C₃₁H₅₂O₅Si₂

Guidance literature:: Multi-step reaction with 15 steps

1.1: 92 percent / H₂SO₄ / Heating

2.1: H₂ / Pd/C / ethanol / 20 °C

2.2: 78 percent / NaNO₂; H₂SO₄ / Heating

3.1: 83 percent / Br₂ / CH₂Cl₂ / -45 °C

4.1: 92 percent / imidazole / dimethylformamide / 20 °C

5.1: 95 percent / diisobutylaluminum hydride / CH₂Cl₂ / -78 °C

6.1: 90 percent / PPTS / CH₂Cl₂ / 20 °C

7.1: n-BuLi / tetrahydrofuran / -78 °C

8.1: NaH / tetrahydrofuran / 20 °C

9.1: 73 percent / CBr₄; PPh₃ / CH₂Cl₂ / 40 °C

10.1: t-BuLi / diethyl ether / -78 °C

10.2: PPh₃ / Pd₂(dba)3 / dimethylformamide / 30 °C

11.1: 85 percent / 1,3-propanedithiol; BF₃*OEt₂ / CH₂Cl₂ / -78 °C

12.1: imidazole / dimethylformamide / 0 °C

13.1: DIBALH / CH₂Cl₂ / -78 °C

14.1: MnO₂ / CH₂Cl₂ / 20 °C

15.1: NaClO₂; NaH₂PO₄; 2-methyl-2-butene / tetrahydrofuran; 2-methyl-propan-2-ol; H₂O / 20 °C

With 1H-imidazole; 1.3-propanedithiol; manganese(IV) oxide; sodium chlorite; sodium dihydrogenphosphate; n-butyllithium; 2-methyl-but-2-ene; carbon tetrabromide; sulfuric acid; boron trifluoride diethyl etherate; hydrogen; bromine; tert.-butyl lithium; pyridinium p-toluenesulfonate; sodium hydride; diisobutylaluminium hydride; triphenylphosphine; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol; 2.2: Sandmeyer reaction / 8.1: Horner-Wadsworth-Emmons reaction / 10.2: Stille reaction / 15.1: Pinnic oxidation;
DOI:10.1016/j.tetlet.2007.05.174