C₁₉H₁₃F₁₃O₄

Base Information

• Chemical Name: C₁₉H₁₃F₁₃O₄
• CAS No.: 1293408-07-7
• Molecular Formula: C₁₉H₁₃F₁₃O₄
• Molecular Weight: 552.289
• Mol file: 1293408-07-7.mol

Synonyms:C₁₉H₁₃F₁₃O₄

Chemical Property of C₁₉H₁₃F₁₃O₄

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of C₁₉H₁₃F₁₃O₄

There total 4 articles about C₁₉H₁₃F₁₃O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

C15H9F13O3 (255041-11-3) + Methacryloyl chloride (920-46-7,26937-45-1) → C19H13F13O4 (1293408-07-7)

Guidance literature:

With triethylamine; In dichloromethane; at 10 - 20 ℃; for 2h; Inert atmosphere;

Reference yield:

C15H9F13O3 (255041-11-3) + methyloxirane (75-56-9,16033-71-9) + Methacryloyl chloride (920-46-7,26937-45-1) → C19H13F13O4 (1293408-07-7) + C22H19F13O5 (1338080-22-0) + C22H19F13O5 (1338080-23-1)

Guidance literature:

C₁₅H₉F₁₃O₃; methyloxirane; With potassium carbonate; In tert-butyl alcohol; at 85 ℃; for 48h;

Methacryloyl chloride; With triethylamine; In acetone; at 10 - 20 ℃; for 15h; Inert atmosphere; Cooling with ice;

Reference yield:

methyl 4-hydroxylbenzoate (99-76-3,156291-94-0) → C19H13F13O4 (1293408-07-7)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / 6 h / 120 °C / Inert atmosphere

2: triethylamine / dichloromethane / 2 h / 10 - 20 °C / Inert atmosphere

With toluene-4-sulfonic acid; triethylamine; In dichloromethane;

upstream raw materials:

C₁₅H₉F₁₃O₃

methyloxirane

Methacryloyl chloride

methyl 4-hydroxylbenzoate

Refernces

• 1、 -. "Fluorinated compound, fluorinated polymer and fluorinated copolymer". . . Retrieved 2013/06/28.