Technology Process of C32H37N7O3
There total 11 articles about C32H37N7O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: potassium carbonate; thiophenol / acetonitrile; dimethyl sulfoxide / 60 °C
2: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C
3: potassium hydroxide; water / methanol / 40 °C
4: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C
5: ammonium acetate / Reflux; Molecular sieve
6: potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0); tricyclohexylphosphine / 1,4-dioxane / 140 °C / Microwave irradiation
7: hydrogenchloride / water; 1,4-dioxane / 50 °C
With
hydrogenchloride; potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0); ammonium acetate; water; potassium carbonate; thiophenol; N-ethyl-N,N-diisopropylamine; potassium hydroxide; tricyclohexylphosphine;
In
1,4-dioxane; methanol; dichloromethane; water; dimethyl sulfoxide; acetonitrile;
6: |Suzuki Coupling;
DOI:10.1002/cmdc.201400045
- Guidance literature:
-
Multi-step reaction with 5 steps
1: potassium hydroxide; water / methanol / 40 °C
2: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C
3: ammonium acetate / Reflux; Molecular sieve
4: potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0); tricyclohexylphosphine / 1,4-dioxane / 140 °C / Microwave irradiation
5: hydrogenchloride / water; 1,4-dioxane / 50 °C
With
hydrogenchloride; potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0); ammonium acetate; water; N-ethyl-N,N-diisopropylamine; potassium hydroxide; tricyclohexylphosphine;
In
1,4-dioxane; methanol; dichloromethane; water;
4: |Suzuki Coupling;
DOI:10.1002/cmdc.201400045