1-Benzo[d]isoxazol-3-yl-cyclohexanecarboxylic acid 3-diethylamino-propyl ester

Base Information

Chemical Name:1-Benzo[d]isoxazol-3-yl-cyclohexanecarboxylic acid 3-diethylamino-propyl ester
CAS No.:110073-52-4
Molecular Formula:C₂₁H₃₀N₂O₃
Molecular Weight:358.481
Hs Code.:

Synonyms:1-Benzo[d]isoxazol-3-yl-cyclohexanecarboxylic acid 3-diethylamino-propyl ester

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Chemical Property of 1-Benzo[d]isoxazol-3-yl-cyclohexanecarboxylic acid 3-diethylamino-propyl ester

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Technology Process of 1-Benzo[d]isoxazol-3-yl-cyclohexanecarboxylic acid 3-diethylamino-propyl ester

There total 5 articles about 1-Benzo[d]isoxazol-3-yl-cyclohexanecarboxylic acid 3-diethylamino-propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 622-93-5
3-diethylamino-propan-1-ol

: 1-Benzo[d]isoxazol-3-yl-cyclohexanecarbonyl chloride

: 110073-52-4
1-Benzo[d]isoxazol-3-yl-cyclohexanecarboxylic acid 3-diethylamino-propyl ester

Guidance literature:: With triethylamine; In toluene; at 100 ℃; for 1h;
DOI:10.1248/cpb.35.2095

Reference yield:

: 111-24-0
1,5-dibromo-pentane

: 110073-52-4
1-Benzo[d]isoxazol-3-yl-cyclohexanecarboxylic acid 3-diethylamino-propyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 15 g / NaH / dimethylsulfoxide

2: NaH / H₂O; ethanol

3: thionyl chloride / toluene / 1 h / 100 °C

4: 33 percent / triethylamine / toluene / 1 h / 100 °C

With thionyl chloride; sodium hydride; triethylamine; In ethanol; water; dimethyl sulfoxide; toluene;
DOI:10.1248/cpb.35.2095

Reference yield:

: 91665-92-8
1-(1,2-benzisoxazol-3-yl)-1-cyclohexanecarboxylic acid

: 110073-52-4
1-Benzo[d]isoxazol-3-yl-cyclohexanecarboxylic acid 3-diethylamino-propyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / toluene / 1 h / 100 °C

2: 33 percent / triethylamine / toluene / 1 h / 100 °C

With thionyl chloride; triethylamine; In toluene;
DOI:10.1248/cpb.35.2095