endo-2-cyano-exo-3,3-di-p-tolyl-anti-8-tert-butoxytricyclo<3.2.1.0^2,4>octane

Base Information

Chemical Name:endo-2-cyano-exo-3,3-di-p-tolyl-anti-8-tert-butoxytricyclo<3.2.1.0^2,4>octane
CAS No.:82521-76-4
Molecular Formula:C₂₇H₃₁NO
Molecular Weight:385.549
Hs Code.:

endo-2-cyano-exo-3,3-di-p-tolyl-anti-8-tert-butoxytricyclo<3.2.1.0<sup>2,4</sup>>octane

Synonyms:endo-2-cyano-exo-3,3-di-p-tolyl-anti-8-tert-butoxytricyclo<3.2.1.0^2,4>octane

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Chemical Property of endo-2-cyano-exo-3,3-di-p-tolyl-anti-8-tert-butoxytricyclo<3.2.1.0^2,4>octane

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Technology Process of endo-2-cyano-exo-3,3-di-p-tolyl-anti-8-tert-butoxytricyclo<3.2.1.0^2,4>octane

There total 5 articles about endo-2-cyano-exo-3,3-di-p-tolyl-anti-8-tert-butoxytricyclo<3.2.1.0^2,4>octane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 82536-73-0
endo-2-cyano-exo-(3,4-diaza-5,5-di-p-tolyl)-anti-10-tert-butoxytricyclo<5.2.1.0^2,6>dec-3-ene

: 82521-76-4
endo-2-cyano-exo-3,3-di-p-tolyl-anti-8-tert-butoxytricyclo<3.2.1.0^2,4>octane

Guidance literature:: In toluene; Heating;
DOI:10.1021/jo00140a026

Reference yield:

: 1143-91-5
bis(4-methylphenyl)diazomethane

: 82521-76-4
endo-2-cyano-exo-3,3-di-p-tolyl-anti-8-tert-butoxytricyclo<3.2.1.0^2,4>octane

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / hydroquinone / diethyl ether / Ambient temperature; 2-3 weeks

2: 91 percent / toluene / Heating

With hydroquinone; In diethyl ether; toluene;
DOI:10.1021/jo00140a026

Reference yield:

: 82521-66-2
2-bromo-anti-7-tert-butoxynorbornene

: 82521-76-4
endo-2-cyano-exo-3,3-di-p-tolyl-anti-8-tert-butoxytricyclo<3.2.1.0^2,4>octane

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / copper(I) cyanide / dimethylformamide / 11 h / Heating

2: 60 percent / hydroquinone / diethyl ether / Ambient temperature; 2-3 weeks

3: 91 percent / toluene / Heating

With copper(l) cyanide; hydroquinone; In diethyl ether; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jo00140a026