(+)-8-penyldeltacyclene

Base Information

Chemical Name:(+)-8-penyldeltacyclene
CAS No.:127256-90-0
Molecular Formula:C₁₅H₁₄
Molecular Weight:194.276
Hs Code.:

Synonyms:(+)-8-penyldeltacyclene

Suppliers and Price of (+)-8-penyldeltacyclene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+)-8-penyldeltacyclene

Chemical Property:

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Technology Process of (+)-8-penyldeltacyclene

There total 5 articles about (+)-8-penyldeltacyclene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.8%

: 121-46-0
bicyclo[2.2.1]hepta-2,5-diene

: 536-74-3
phenylacetylene

: 68886-18-0,127256-90-0,127279-29-2
4-phenyldeltacyclen

Guidance literature:: With diphosphane; (2S,3S)-(+)-bis(diphenylphosphanyl)bicyclo[2.2.1]hept-5-ene; cobalt(III) acetylacetonate; diethylaluminium chloride; In tetrahydrofuran; hexane; at 35 ℃; for 3h; Product distribution; other alkynes; other optical active reagents; var. reaction time;
DOI:10.1016/0022-328X(91)86338-Q

Reference yield:

: 121-46-0
bicyclo[2.2.1]hepta-2,5-diene

: 536-74-3
phenylacetylene

: 127279-29-2
C₁₅H₁₄

: 127256-90-0
C₁₅H₁₄

Guidance literature:: (1S,2R,3R,4R)-(-)-2,3-bis(diphenylphosphane)bicyclo[2.2.1]hept-5-ene; In tetrahydrofuran; at 35 ℃; for 4h;

Reference yield:

: 121-46-0
bicyclo[2.2.1]hepta-2,5-diene

: 536-74-3
phenylacetylene

: 68886-18-0,127256-90-0,127279-29-2
4-phenyldeltacyclen

: 68886-18-0,127256-90-0,127279-29-2
4-phenyldeltacyclen

Guidance literature:: With diphosphane; cobalt(III) acetylacetonate; R-Prophos; diethylaluminium chloride; In tetrahydrofuran; at 35 ℃; for 4h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1016/0022-328X(91)86338-Q