C₂₀H₁₉NO₁₀

Base Information

• Chemical Name: C₂₀H₁₉NO₁₀
• CAS No.: 161391-08-8
• Molecular Formula: C₂₀H₁₉NO₁₀
• Molecular Weight: 433.372
• Mol file: 161391-08-8.mol

Synonyms:C₂₀H₁₉NO₁₀

Chemical Property of C₂₀H₁₉NO₁₀

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₀H₁₉NO₁₀

There total 1 articles about C₂₀H₁₉NO₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

C26H24N2O9 (161391-07-7) → C20H19NO10 (161391-08-8)

Guidance literature:

With boron trifluoride diethyl etherate; acetic acid; ethyl acetate; In dichloromethane; 1.) 0 deg C to 25 deg C, 0.3 h; 2.) 25 deg C, 0.6 h;

DOI:10.1016/S0040-4020(01)89281-4

Reference yield:

C20H19NO10 (161391-08-8) → C26H30N2O9 (161391-12-4)

Guidance literature:

Multi-step reaction with 4 steps

1: PPTS / CHCl₃ / 16 h / Heating

2: 92 percent / t-butyl lithium / pentane; tetrahydrofuran / 0.1 h / -78 °C

3: 82 percent / triethylamine, DMAP, acetic anhydride / CH₂Cl₂ / 120 h / 25 °C

4: 80 percent / lithium hydride, ethylene glycol / tetrahydrofuran / 1.25 h / 25 °C

With dmap; tert.-butyl lithium; pyridinium p-toluenesulfonate; acetic anhydride; lithium hydride; ethylene glycol; triethylamine; In tetrahydrofuran; dichloromethane; chloroform; pentane;

DOI:10.1016/S0040-4020(01)89281-4

Reference yield:

C20H19NO10 (161391-08-8) → C26H28N2O9 (161391-13-5)

Guidance literature:

Multi-step reaction with 5 steps

1: PPTS / CHCl₃ / 16 h / Heating

2: 92 percent / t-butyl lithium / pentane; tetrahydrofuran / 0.1 h / -78 °C

3: 82 percent / triethylamine, DMAP, acetic anhydride / CH₂Cl₂ / 120 h / 25 °C

4: 80 percent / lithium hydride, ethylene glycol / tetrahydrofuran / 1.25 h / 25 °C

5: 93 percent / Dess Martin periodinane / acetonitrile / 30 h / 25 °C

With dmap; tert.-butyl lithium; pyridinium p-toluenesulfonate; acetic anhydride; lithium hydride; Dess-Martin periodane; ethylene glycol; triethylamine; In tetrahydrofuran; dichloromethane; chloroform; acetonitrile; pentane;

DOI:10.1016/S0040-4020(01)89281-4

upstream raw materials:

C₂₆H₂₄N₂O₉

Downstream raw materials:

C₂₆H₃₀N₂O₉

C₂₆H₂₈N₂O₉

C₂₇H₂₈N₂O₁₀

C₂₉H₃₆N₂O₉Si