Technology Process of C17H18N4O2S
There total 10 articles about C17H18N4O2S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C22H28N4O5S;
With
sulfuric acid;
In
water;
at 80 ℃;
for 0.333333h;
With
sodium hydroxide;
In
water;
pH=8;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium tetrahydroborate; methanol / 1 h / -10 - 0 °C
2.1: methyllithium / tetrahydrofuran / 2.5 h / -78 °C / Inert atmosphere
3.1: potassium phosphate / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide; water / 0.5 h / 100 °C
4.1: sodium tetrahydroborate; methanol / 1 h / 20 °C
5.1: sulfuric acid / water / 0.33 h / 80 °C
5.2: pH 8
With
methanol; sodium tetrahydroborate; potassium phosphate; sulfuric acid; methyllithium;
bis-triphenylphosphine-palladium(II) chloride;
In
tetrahydrofuran; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: methyllithium / tetrahydrofuran / 2.5 h / -78 °C / Inert atmosphere
2.1: potassium phosphate / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide; water / 0.5 h / 100 °C
3.1: sodium tetrahydroborate; methanol / 1 h / 20 °C
4.1: sulfuric acid / water / 0.33 h / 80 °C
4.2: pH 8
With
methanol; sodium tetrahydroborate; potassium phosphate; sulfuric acid; methyllithium;
bis-triphenylphosphine-palladium(II) chloride;
In
tetrahydrofuran; water; N,N-dimethyl-formamide;
