C₁₂₀H₁₂₀Br₆O₁₂S₃

Base Information

• Chemical Name: C₁₂₀H₁₂₀Br₆O₁₂S₃
• CAS No.: 1358597-29-1
• Molecular Formula: C₁₂₀H₁₂₀Br₆O₁₂S₃
• Molecular Weight: 2329.89
• Mol file: 1358597-29-1.mol

Synonyms:C₁₂₀H₁₂₀Br₆O₁₂S₃

Chemical Property of C₁₂₀H₁₂₀Br₆O₁₂S₃

Chemical Property:

Purity/Quality:

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Technology Process of C₁₂₀H₁₂₀Br₆O₁₂S₃

There total 1 articles about C₁₂₀H₁₂₀Br₆O₁₂S₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

C99H102Br6O6 (1358597-28-0) + p-toluenesulfonyl chloride (98-59-9) → C120H120Br6O12S3 (1358597-29-1)

Guidance literature:

With dmap; triethylamine; In dichloromethane; at 20 ℃; for 5h; Cooling;

DOI:10.1039/c1jm14138d

Reference yield: 73.0%

C120H120Br6O12S3 (1358597-29-1) + methyl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzoate (171364-80-0) → C168H162O24S3

Guidance literature:

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium carbonate; tricyclohexylphosphine; In tetrahydrofuran; water; for 20h; Inert atmosphere; Reflux;

DOI:10.1039/c1jm14138d

upstream raw materials:

C₉₉H₁₀₂Br₆O₆

p-toluenesulfonyl chloride