N-(3-(10,11-dihydro-5H-dibenzo[a,d][7]annulen-5-ylidene)propyl)-4-cyanobenzenesulfonamide

Base Information

Chemical Name:N-(3-(10,11-dihydro-5H-dibenzo[a,d][7]annulen-5-ylidene)propyl)-4-cyanobenzenesulfonamide
CAS No.:1423077-90-0
Molecular Formula:C₂₅H₂₂N₂O₂S
Molecular Weight:414.528
Hs Code.:

Synonyms:N-(3-(10,11-dihydro-5H-dibenzo[a,d][7]annulen-5-ylidene)propyl)-4-cyanobenzenesulfonamide

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Chemical Property of N-(3-(10,11-dihydro-5H-dibenzo[a,d][7]annulen-5-ylidene)propyl)-4-cyanobenzenesulfonamide

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Technology Process of N-(3-(10,11-dihydro-5H-dibenzo[a,d][7]annulen-5-ylidene)propyl)-4-cyanobenzenesulfonamide

There total 3 articles about N-(3-(10,11-dihydro-5H-dibenzo[a,d][7]annulen-5-ylidene)propyl)-4-cyanobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 25887-71-2
3-(10,11-dihydro-5H-dibenzo[a,d][7]annulen-5-ylidene)propan-1-amine hydrochloride

: 49584-26-1
p-cyanobenzenesulfonyl chloride

: 1423077-90-0
N-(3-(10,11-dihydro-5H-dibenzo[a,d][7]annulen-5-ylidene)propyl)-4-cyanobenzenesulfonamide

Guidance literature:: With p-toluenesulfonyl chloride; In N,N-dimethyl-formamide; at 0 - 25 ℃; for 2h;

Reference yield:

: 1423078-16-3
5-(3-azidopropylidene)-10,11-dihydro-5H-dibenzo[a,d][7]annulene

: 1423077-90-0
N-(3-(10,11-dihydro-5H-dibenzo[a,d][7]annulen-5-ylidene)propyl)-4-cyanobenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: triphenylphosphine / tetrahydrofuran / 2 h / 0 - 25 °C

2: p-toluenesulfonyl chloride / N,N-dimethyl-formamide / 2 h / 0 - 25 °C

With p-toluenesulfonyl chloride; triphenylphosphine; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

: 3436-04-2
5-(3-bromo-1-propylidene)-10,11-dihydro-5H-dibenzo[a,d]cycloheptene

: 1423077-90-0
N-(3-(10,11-dihydro-5H-dibenzo[a,d][7]annulen-5-ylidene)propyl)-4-cyanobenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium azide / N,N-dimethyl-formamide / 14 h / 25 °C

2: triphenylphosphine / tetrahydrofuran / 2 h / 0 - 25 °C

3: p-toluenesulfonyl chloride / N,N-dimethyl-formamide / 2 h / 0 - 25 °C

With sodium azide; p-toluenesulfonyl chloride; triphenylphosphine; In tetrahydrofuran; N,N-dimethyl-formamide;