Technology Process of C34H26F4N4O5
There total 14 articles about C34H26F4N4O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 10 steps
1: tetrahydrofuran
2: Py / CH2Cl2
3: LiCl / dimethylformamide
4: NH4COOH / Pd/C / tetrahydrofuran; methanol
5: HCl / ethyl acetate
6: 91 percent / N-(3-(dimethylamino)propyl)-N'-ethylcarbodiimide hydrochloride / various solvent(s) / 5 h
7: HCl / ethyl acetate
8: various solvent(s) / 3 h
9: Et3N, H2O / acetonitrile / 1 h
10: Et3N / various solvent(s) / 1 h
With
pyridine; hydrogenchloride; water; ammonium formate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; lithium chloride;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ja9703133
- Guidance literature:
-
Multi-step reaction with 9 steps
1: Py / CH2Cl2
2: LiCl / dimethylformamide
3: NH4COOH / Pd/C / tetrahydrofuran; methanol
4: HCl / ethyl acetate
5: 91 percent / N-(3-(dimethylamino)propyl)-N'-ethylcarbodiimide hydrochloride / various solvent(s) / 5 h
6: HCl / ethyl acetate
7: various solvent(s) / 3 h
8: Et3N, H2O / acetonitrile / 1 h
9: Et3N / various solvent(s) / 1 h
With
pyridine; hydrogenchloride; water; ammonium formate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; lithium chloride;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ja9703133
- Guidance literature:
-
Multi-step reaction with 8 steps
1: LiCl / dimethylformamide
2: NH4COOH / Pd/C / tetrahydrofuran; methanol
3: HCl / ethyl acetate
4: 91 percent / N-(3-(dimethylamino)propyl)-N'-ethylcarbodiimide hydrochloride / various solvent(s) / 5 h
5: HCl / ethyl acetate
6: various solvent(s) / 3 h
7: Et3N, H2O / acetonitrile / 1 h
8: Et3N / various solvent(s) / 1 h
With
hydrogenchloride; water; ammonium formate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; lithium chloride;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ja9703133