1,1,7,7-Tetrachloro-3,3,4,4,5,5-hexafluoro-1,7-diphenyl-heptane-2,6-dione

Base Information

• Chemical Name: 1,1,7,7-Tetrachloro-3,3,4,4,5,5-hexafluoro-1,7-diphenyl-heptane-2,6-dione
• CAS No.: 94219-86-0
• Molecular Formula: C₁₉H₁₀Cl₄F₆O₂
• Molecular Weight: 526.09

Synonyms:1,1,7,7-Tetrachloro-3,3,4,4,5,5-hexafluoro-1,7-diphenyl-heptane-2,6-dione

Chemical Property of 1,1,7,7-Tetrachloro-3,3,4,4,5,5-hexafluoro-1,7-diphenyl-heptane-2,6-dione

Chemical Property:

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Technology Process of 1,1,7,7-Tetrachloro-3,3,4,4,5,5-hexafluoro-1,7-diphenyl-heptane-2,6-dione

There total 2 articles about 1,1,7,7-Tetrachloro-3,3,4,4,5,5-hexafluoro-1,7-diphenyl-heptane-2,6-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

diethyl perfluoroglutarate (424-40-8) + (α,α-dichlorobenzyl)lithium (3141-47-7) → 1,1,7,7-Tetrachloro-3,3,4,4,5,5-hexafluoro-1,7-diphenyl-heptane-2,6-dione (94219-86-0)

Guidance literature:

In tetrahydrofuran; diethyl ether; hexane; at -115 ℃; for 7h;

DOI:10.1016/S0022-1139(00)80929-X

Reference yield:

Benzotrichlorid (98-07-7) → 1,1,7,7-Tetrachloro-3,3,4,4,5,5-hexafluoro-1,7-diphenyl-heptane-2,6-dione (94219-86-0)

Guidance literature:

Multi-step reaction with 2 steps

1: n-C₄H₉Li / diethyl ether; tetrahydrofuran; hexane / 1.5 h / -115 °C

2: 85 percent / diethyl ether; tetrahydrofuran; hexane / 7 h / -115 °C

With n-butyllithium; In tetrahydrofuran; diethyl ether; hexane;

DOI:10.1016/S0022-1139(00)80929-X

Reference yield: 90.0%

diethylperfluoro-6,11-dioxahexadecanedioate (61210-88-6) + 1,1,7,7-Tetrachloro-3,3,4,4,5,5-hexafluoro-1,7-diphenyl-heptane-2,6-dione (94219-86-0) → 1,1-Dichloro-6-[4-(6,6-dichloro-1,1,2,2,3,3,4,4-octafluoro-5-oxo-6-phenyl-hexyloxy)-1,1,2,2,3,3,4,4-octafluoro-butoxy]-3,3,4,4,5,5,6,6-octafluoro-1-phenyl-hexan-2-one

Guidance literature:

In tetrahydrofuran; diethyl ether; hexane; at -115 ℃; for 1.5h;

DOI:10.1016/S0022-1139(00)80929-X

upstream raw materials:

diethyl perfluoroglutarate

(α,α-dichlorobenzyl)lithium

Benzotrichlorid

Downstream raw materials:

3,3,4,4,5,5-Hexafluoro-1,7-diphenyl-heptane-1,2,6,7-tetraone

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