2-[(S)-1-(2-{5-[(R)-2-(8-benzyloxy-2-oxo-1,2-dihydroquinolin-5-yl)-2-(tert-butyldimethylsilanyloxy)ethylamino]pentylsulfamoyl}ethyl)pyrrolidin-3-yl]-2,2-diphenylacetamide

Base Information

• Chemical Name: 2-[(S)-1-(2-{5-[(R)-2-(8-benzyloxy-2-oxo-1,2-dihydroquinolin-5-yl)-2-(tert-butyldimethylsilanyloxy)ethylamino]pentylsulfamoyl}ethyl)pyrrolidin-3-yl]-2,2-diphenylacetamide
• CAS No.: 1361952-76-2
• Molecular Formula: C₄₉H₆₅N₅O₆SSi
• Molecular Weight: 880.237

Synonyms:2-[(S)-1-(2-{5-[(R)-2-(8-benzyloxy-2-oxo-1,2-dihydroquinolin-5-yl)-2-(tert-butyldimethylsilanyloxy)ethylamino]pentylsulfamoyl}ethyl)pyrrolidin-3-yl]-2,2-diphenylacetamide

Chemical Property of 2-[(S)-1-(2-{5-[(R)-2-(8-benzyloxy-2-oxo-1,2-dihydroquinolin-5-yl)-2-(tert-butyldimethylsilanyloxy)ethylamino]pentylsulfamoyl}ethyl)pyrrolidin-3-yl]-2,2-diphenylacetamide

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Technology Process of 2-[(S)-1-(2-{5-[(R)-2-(8-benzyloxy-2-oxo-1,2-dihydroquinolin-5-yl)-2-(tert-butyldimethylsilanyloxy)ethylamino]pentylsulfamoyl}ethyl)pyrrolidin-3-yl]-2,2-diphenylacetamide

There total 1 articles about 2-[(S)-1-(2-{5-[(R)-2-(8-benzyloxy-2-oxo-1,2-dihydroquinolin-5-yl)-2-(tert-butyldimethylsilanyloxy)ethylamino]pentylsulfamoyl}ethyl)pyrrolidin-3-yl]-2,2-diphenylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(R)-8-(benzyloxy)-5-(2-bromo-1-((tert-butyldimethylsilyl)oxy)ethyl)quinolin-2(1H)-one (530084-74-3) + 2-{(S)-1-[2-(5-aminopentylsulfamoyl)ethyl]pyrrolidin-3-yl}-2,2-diphenylacetamide → 2-[(S)-1-(2-{5-[(R)-2-(8-benzyloxy-2-oxo-1,2-dihydroquinolin-5-yl)-2-(tert-butyldimethylsilanyloxy)ethylamino]pentylsulfamoyl}ethyl)pyrrolidin-3-yl]-2,2-diphenylacetamide (1361952-76-2)

Guidance literature:

In dimethyl sulfoxide; at 20 - 90 ℃; for 8h;

Reference yield:

2-[(S)-1-(2-{5-[(R)-2-(8-benzyloxy-2-oxo-1,2-dihydroquinolin-5-yl)-2-(tert-butyldimethylsilanyloxy)ethylamino]pentylsulfamoyl}ethyl)pyrrolidin-3-yl]-2,2-diphenylacetamide (1361952-76-2) → 2-[(S)-1-(2-{5-[(R)-2-(8-benzyloxy-2-oxo-1,2-dihydroquinolin-5-yl)-2-hydroxy-ethylamino]pentylsulfamoyl}ethyl)pyrrolidin-3-yl]-2,2-diphenylacetamide (1361952-77-3)

Guidance literature:

With triethylamine tris(hydrogen fluoride); In dichloromethane; for 10h;

upstream raw materials:

(R)-8-(benzyloxy)-5-(2-bromo-1-((tert-butyldimethylsilyl)oxy)ethyl)quinolin-2(1H)-one

Downstream raw materials:

2-[(S)-1-(2-{5-[(R)-2-(8-benzyloxy-2-oxo-1,2-dihydroquinolin-5-yl)-2-hydroxy-ethylamino]pentylsulfamoyl}ethyl)pyrrolidin-3-yl]-2,2-diphenylacetamide

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