(E)-3',4'-dimethoxy-2'-(3,4-dimethoxycinnamoyloxy)acetophenone

Base Information

• Chemical Name: (E)-3',4'-dimethoxy-2'-(3,4-dimethoxycinnamoyloxy)acetophenone
• CAS No.: 1196971-27-3
• Molecular Formula: C₂₁H₂₂O₇
• Molecular Weight: 386.401
• Mol file: 1196971-27-3.mol

Synonyms:(E)-3',4'-dimethoxy-2'-(3,4-dimethoxycinnamoyloxy)acetophenone

Chemical Property of (E)-3',4'-dimethoxy-2'-(3,4-dimethoxycinnamoyloxy)acetophenone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of (E)-3',4'-dimethoxy-2'-(3,4-dimethoxycinnamoyloxy)acetophenone

There total 1 articles about (E)-3',4'-dimethoxy-2'-(3,4-dimethoxycinnamoyloxy)acetophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

2'-hydroxy-3',4'-dimethoxyacetophenone (5396-18-9) + 3,4-dimethoxycinnamic acid (2316-26-9) → (E)-3',4'-dimethoxy-2'-(3,4-dimethoxycinnamoyloxy)acetophenone (1196971-27-3)

Guidance literature:

With 4-pyrrolidin-1-ylpyridine; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 18h; Inert atmosphere;

DOI:10.1016/j.bmc.2009.08.056

Reference yield: 62.0%

(E)-3',4'-dimethoxy-2'-(3,4-dimethoxycinnamoyloxy)acetophenone (1196971-27-3) → 3-hydroxy-1-(2-hydroxy-3,4-dimethoxyphenyl)-5-(3,4-dimethoxyphenyl)penta-2,4-dien-1-one (1196971-30-8)

Guidance literature:

(E)-3',4'-dimethoxy-2'-(3,4-dimethoxycinnamoyloxy)acetophenone; With potassium hydroxide; In dimethyl sulfoxide; at 20 ℃; for 2h; Inert atmosphere;

With hydrogenchloride; In water; dimethyl sulfoxide; pH=4;

DOI:10.1016/j.bmc.2009.08.056

upstream raw materials:

2'-hydroxy-3',4'-dimethoxyacetophenone

3,4-dimethoxycinnamic acid

Downstream raw materials:

3-hydroxy-1-(2-hydroxy-3,4-dimethoxyphenyl)-5-(3,4-dimethoxyphenyl)penta-2,4-dien-1-one