dicarbonyl(3-hydroxy-3,5,5-trimethyl-1-penten-1,1-diyl)bis(trimethylphosphite)iron⁽⁰⁾

Base Information

• Chemical Name: dicarbonyl(3-hydroxy-3,5,5-trimethyl-1-penten-1,1-diyl)bis(trimethylphosphite)iron⁽⁰⁾
• CAS No.: 198136-53-7
• Molecular Formula: C₁₆H₃₂FeO₉P₂
• Molecular Weight: 486.219

Synonyms:dicarbonyl(3-hydroxy-3,5,5-trimethyl-1-penten-1,1-diyl)bis(trimethylphosphite)iron⁽⁰⁾

Chemical Property of dicarbonyl(3-hydroxy-3,5,5-trimethyl-1-penten-1,1-diyl)bis(trimethylphosphite)iron⁽⁰⁾

Chemical Property:

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Technology Process of dicarbonyl(3-hydroxy-3,5,5-trimethyl-1-penten-1,1-diyl)bis(trimethylphosphite)iron⁽⁰⁾

There total 1 articles about dicarbonyl(3-hydroxy-3,5,5-trimethyl-1-penten-1,1-diyl)bis(trimethylphosphite)iron⁽⁰⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

3,4,4-trimethylpent-1-yn-3-ol (38484-41-2,38484-42-3,104758-84-1,993-53-3) + Na(1+)*FeI(CO)2(P(OCH3)3)2(1-) = Na[FeI(CO)2(P(OCH3)3)2] → dicarbonylbis(trimethyl phosphite)vinylideneiron(0) (187849-63-4) + dicarbonyl(3-hydroxy-3,5,5-trimethyl-1-penten-1,1-diyl)bis(trimethylphosphite)iron(0) (198136-53-7)

Guidance literature:

In tetrahydrofuran; byproducts: benzophenone; N2-atmosphere; addn. of 1.5 equiv. of alkyne to Fe-complex soln. at -30°C, warming to room temp.; solvent removal, dissoln. in hexane, chromy. (SiO2, hexane/ether=50:1), evapn.; elem. anal.;

DOI:10.1016/S0022-328X(97)00012-0

upstream raw materials:

3,4,4-trimethylpent-1-yn-3-ol

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